{"title":"Distillation \u0026 Recovery","description":null,"products":[{"product_id":"2l-standard-short-path-parts-kit","title":"BVV - 2L Standard Short Path Parts Kit","description":"\u003ch2\u003eShort Path Distillation Setup\u003c\/h2\u003e \u003cbr\u003e \u003cp\u003e\u003cimg title=\"Distillation Flow Chart\" alt=\"Distillation Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_distillationdiagramfinal_jpg?632197998369606337\" width=\"900\"\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003e\u003ciframe width=\"560\" height=\"315\" src=\"https:\/\/www.youtube.com\/embed\/U6A7zofqvWo\" frameborder=\"0\" allow=\"accelerometer; autoplay; encrypted-media; gyroscope; picture-in-picture\" allowfullscreen=\"\"\u003e\u003c\/iframe\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003eShort path distillation is used for compounds that are not stable at high temperatures. It can also be used to purify small amounts of a compound.\u003c\/span\u003e\u003c\/p\u003e \u003cp\u003eThe 2L Distillation Kit gives users an easy to use system that will get them up and running at an affordable price. It includes all stands, clamps, clips,\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cem\u003eThis Kit Does NOT include a vacuum pump, circulator, or heating source. Please see the below recommendations for both as well as recommended add-ons. Or check out our \u003ca title=\"2L Standard Short Path Distillation Turnkey Setup\" href=\"https:\/\/shopbvv.com\/products\/2l-standard-short-path-distillation-turnkey-setup\"\u003e2L Standard Distillation Turnkey Setup\u003c\/a\u003e which includes vacuum pump, circulator, and mantle.\u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e \u003ch3\u003e\u003cstrong\u003eRecommended Vacuum Pumps: \u003c\/strong\u003e\u003c\/h3\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePro Series 5.6CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eJust Better 6 CFM 2 Stage Deep Vacuum Pump (economy option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBest Value Vacs VE280 9CFM Two Stage Vacuum Pump (economy option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003ch3\u003e\u003cstrong\u003eRecommended Circulators:\u003c\/strong\u003e\u003c\/h3\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePolyscience 7 Liter MX Heated Circulator (economy option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePolyscience 7 Liter MX Refrigerated Circulator (premium option with chilling capability)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003ch3\u003e\u003cstrong\u003eRecommended Heating Mantle:\u003c\/strong\u003e\u003c\/h3\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003ca href=\"https:\/\/shopbvv.com\/products\/2l-digital-heating-and-stirring-mantle\" target=\"_blank\"\u003eBVV 2L Heating Mantle\u003c\/a\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003ch3\u003e\u003cstrong\u003eRecommended Add-Ons: \u003c\/strong\u003e\u003c\/h3\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eGlass Dewar Style Cold Trap (recommended cold trap)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBullseye Precison Vacuum Gauge (premium vacuum gauge for measuring depth)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eCT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003ch2\u003e\u003cstrong\u003eShort Path Distillation Kit Specifications:\u003c\/strong\u003e\u003c\/h2\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBoiling Flask Size: 2L\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRecieving Flask Size: 250ml\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBatch Capacity approximate: 2L = 400-1000 grams\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRun time: 4 to 8 hours dependent upon material composition and throughput\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDistillation Temperature Range: 140-250C (Do not exceed 250C)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRecommended Condenser Temperature: 40-50C\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003ch3\u003e\u003cstrong\u003eThis Kit Comes Standard With The Following:\u003c\/strong\u003e\u003c\/h3\u003e \u003cp\u003e\u003cem\u003eGlass Components:\u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e2L 2-Neck Boiling Flask\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eShort Path Head\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTriple Neck Cow\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e3x 250mL Single Neck Receiving Flask\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1\/8\" 14\/20 PTFE Thermometer Adapter\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1\/4\" 24\/40 PTFE Thermometer Adapter\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e120mm Glass Funnel\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cem\u003eAccessories:\u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eMagnetic PTFE Stirring Bar Retriever\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eKeck Clips\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e3 Finger Clamp Adjustable 0-70mm\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBoss head\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e6\" x 6\" Scissor Jack\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e250-500ml Cork Stand\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTraceable Kangaroo Thermometer - Digital\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003ch2\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/h2\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs.\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e \u003ca title=\"Vacuum Pumps\" href=\"https:\/\/shopbvv.com\/collections\/vacuum-pumps\"\u003eVacuum Pump\u003c\/a\u003e is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003cli\u003eOnce process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003eLearn more about short path distillation components and FAQs with \u003ca title=\"Short Path Distillation Guide\" href=\"https:\/\/shopbvv.com\/blogs\/bvv-resources\/short-path-distillation-basics\"\u003ethis distillation guide\u003c\/a\u003e.\u003cbr\u003e\u003c\/p\u003e \u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cspan\u003e*Notice to \u003c\/span\u003e\u003cspan\u003eCustomers\u003c\/span\u003e\u003cspan\u003e: All units are inspected for broken glassware or parts before leaving BVV. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer\u003c\/span\u003e\u003cspan\u003e \u003c\/span\u003e\u003cem\u003e\u003cstrong\u003eMUST contact BVV within 72 hours from carrier delivery to file a claim\u003c\/strong\u003e.\u003c\/em\u003e\u003cspan\u003e If the customer DOES NOT contact BVV within 72 hours from carrier delivery, then BVV cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. \u003c\/span\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cspan\u003eBVV is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.\u003c\/span\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567486116151,"sku":"SP-2LPK-B","price":475.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/d8e1ba2cc1734d4357bf6b64b3e4a851.jpg?v=1758128270"},{"product_id":"magnetic-ptfe-stirring-bar-l-style-70mm","title":"BVV - Magnetic PTFE Stirring Bar - L Style - 70mm","description":"\u003ch2\u003eMagnetic PTFE Stir Bar - L Style - 70mm\u003c\/h2\u003e \u003cp\u003eReduce stir bar jumping with the contoured shape of this L Style Magnetic PTFE Stir Bar. Ideal for round-bottom flask stirring applications. This 70mm L Style Magnetic Stir bar is great for round-bottom flasks above 5 liters in capacity. With its PTFE coating this Magnetic Stir Bar carries excellent solvent and temperature compatibility for a variety of applications.\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eSpecifications:\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eL Style\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e70mm Length\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eMaterial: High-temperature PTFE\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567489851703,"sku":"L70","price":15.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/2cdc53802ce1c1dce20cbf0b0a19e892.jpg?v=1758128384"},{"product_id":"50l-turnkey-reactor-kit","title":"BVV - 50L Turnkey Reactor Kit","description":"\u003ch2\u003e\u003cspan\u003e50L Turnkey Reactor Kit\u003c\/span\u003e\u003c\/h2\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003eThe BVV 50L Double Jacketed Glass Reactor Kit is the ideal solution for small to medium-sized solvent recovery and decarboxylation applications. This kit includes everything to get you up and running including a Single 50L triple-layer Glass Reactor with Condenser, \u003cspan\u003eeither a BVV 19L Heated circulator capable of heating to 220C or \u003c\/span\u003ea UL-listed Huber T305 Capable of heating up to 300C, a 1HP Polyscience 6160T for chilling the condenser, a Welch BTpro100 for vacuum, 25ft of 3\/8\" Gum rubber tubing for vacuum connections, 20ft of reinforced PVC hose for the chiller, 1\/2\" Stainless Steel JIC Hoses for the heater, 5 Gallons of Therminol Heat transfer fluid and 5 Gallons of Propylene glycol.\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cul\u003e\u003c\/ul\u003e \u003cp\u003e\u003cstrong\u003e50L Double Jacketed Glass Reactor Specifications\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003eGlass Material: GG-17 High Borosilicate Glass\u003c\/li\u003e \u003cli\u003eInternal Volume: 50L\u003cbr\u003e \u003c\/li\u003e \u003cli\u003e10.5L Jacket Capacity\u003c\/li\u003e \u003cli\u003eShelf Material: Aluminum Alloy\u003c\/li\u003e \u003cli\u003eHomogenizer Power: 110V\/60Hz\u003c\/li\u003e \u003cli\u003eHomogenizer Speed: 0-400 RPM\u003c\/li\u003e \u003cli\u003eDigital Homogenizer Control\u003c\/li\u003e \u003cli\u003eDigital temperature probe readout included\u003c\/li\u003e \u003cli\u003eDouble Jacket\u003c\/li\u003e \u003cli\u003e3\/4\" Jacket Connections\u003c\/li\u003e \u003cli\u003e1\/4\" and 3\/8\" Vacuum Connections\u003c\/li\u003e \u003cli\u003eLength: 24 in.\u003c\/li\u003e \u003cli\u003eWidth: 30 in.\u003c\/li\u003e \u003cli\u003eHeight: 90 in.\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003cstrong\u003ePolyscience 6100 1 HP Chiller Specifications\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003e6100 Series 1 HP Chiller with Turbine Pump, 100psi; 13.2l\/min\u003c\/li\u003e \u003cli\u003eDisplay: LED\u003c\/li\u003e \u003cli\u003eWorking Temperature Range C: -10 to 40\u003c\/li\u003e \u003cli\u003eTemperature Stability: +\/-0.1\u003c\/li\u003e \u003cli\u003eTemperature Calibration Capability: 1-point\u003c\/li\u003e \u003cli\u003ePump Type: Turbine\u003c\/li\u003e \u003cli\u003eWorking Temperature Range F: 14 to 104\u003c\/li\u003e \u003cli\u003eWorking Temperature Range C: -10 to 40\u003c\/li\u003e \u003cli\u003eReservoir Capacity (gallons): 1.11\u003c\/li\u003e \u003cli\u003eReservoir Capacity (liters): 4.2\u003c\/li\u003e \u003cli\u003eReservoir Cover: Screw-on cap\u003c\/li\u003e \u003cli\u003eCleanable Air Filter: Yes\u003c\/li\u003e \u003cli\u003eCleanable Fluid Filter: Yes\u003c\/li\u003e \u003cli\u003eTemperature Stability F: +\/-0.2\u003c\/li\u003e \u003cli\u003eTemperature Stability C: +\/-0.1\u003c\/li\u003e \u003cli\u003eDisplay: LED\u003c\/li\u003e \u003cli\u003eDisplay Resolution (Read): 0.1\u003c\/li\u003e \u003cli\u003ePump Type: Turbine\u003c\/li\u003e \u003cli\u003eProcess Connections: 1\/2\" FNPT\u003c\/li\u003e \u003cli\u003eOver-Temperature Protection \/ Failsafe Heater Control: Yes\u003c\/li\u003e \u003cli\u003eReservoir Liquid Level Indicator: Yes\u003c\/li\u003e \u003cli\u003eReservoir Drain: Yes\u003c\/li\u003e \u003cli\u003eCool Command Refrigeration Technology: Yes\u003c\/li\u003e \u003cli\u003eWhisperCool Environmental Control Technology: Yes\u003c\/li\u003e \u003cli\u003eMaximum Ambient Temperature F: 95\u003c\/li\u003e \u003cli\u003eMaximum Ambient Temperature C: 35\u003c\/li\u003e \u003cli\u003eOverall Dimensions (LxWxH inches): 27.6 x 14.5 x 22.6\u003c\/li\u003e \u003cli\u003eOverall Dimensions (LxWxH cm): 70 x 36.8 x 57.5\u003c\/li\u003e \u003cli\u003eCompressor Size (HP): 1\u003c\/li\u003e \u003cli\u003eRefrigerant: R134a\u003c\/li\u003e \u003cli\u003eShipping Weight (pounds): 199\u003c\/li\u003e \u003cli\u003eShipping Weight (kilograms): 90\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003cstrong\u003eWelch BTpro100 Specifications\u003c\/strong\u003e\u003c\/p\u003e \u003ctable\u003e \u003cthead\u003e \u003ctr\u003e \u003cth\u003eModel\u003c\/th\u003e \u003cth\u003eBTpro100\u003c\/th\u003e \u003c\/tr\u003e \u003c\/thead\u003e \u003ccolgroup\u003e \u003ccol\u003e \u003ccol\u003e \u003c\/colgroup\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd\u003eFree Air Displacement@60Hz,\u003cbr\u003elpm(CFM)\u003c\/td\u003e \u003ctd\u003e100(3.5)\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eUltimate Vacuum Pressure, Torr\u003c\/td\u003e \u003ctd\u003e6\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eMaximum Vacuum, in. Hg\u003c\/td\u003e \u003ctd\u003e29.7\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eHorsepower, HP (watts)\u003c\/td\u003e \u003ctd\u003e0.5(390)\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eBuilt-in adjustable vacuum\u003c\/td\u003e \u003ctd\u003e-\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eGas Ballast\u003c\/td\u003e \u003ctd\u003eYes\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eHead Material\u003c\/td\u003e \u003ctd\u003ePTFE\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eDiaphragm\u003c\/td\u003e \u003ctd\u003ePTFE\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eInlet\/outlet Connection\u003c\/td\u003e \u003ctd\u003e \u003cp\u003eNW16 flange\u003csup\u003e1\u003c\/sup\u003e\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eAgency (National Recognized Lab)\u003c\/td\u003e \u003ctd\u003ecUL\u003cbr\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eWeight, lbs (kg)\u003c\/td\u003e \u003ctd\u003e40.3(18.3)\u003cbr\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eOverall Dimensions\u003cbr\u003e\u003cbr\u003e\u003cbr\u003eLxWxH in.(cm)\u003c\/td\u003e \u003ctd\u003e9x15x7\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e(23x38x18)\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eShipping Weight, lbs(kg)\u003c\/td\u003e \u003ctd\u003e48.5 (22)\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eShipping Carton Dimensions\u003cbr\u003e\u003cbr\u003e\u003cbr\u003eLxWxH in.(cm)\u003c\/td\u003e \u003ctd\u003e18.9x12.6x11.8\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e(48x32x30)\u003cbr\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003cstrong\u003eHUBER T305 Specifications\u003c\/strong\u003e\u003c\/p\u003e \u003ctable\u003e \u003cthead\u003e \u003ctr\u003e \u003cth colspan=\"2\"\u003e\u003cspan\u003eGeneral Information \u0026amp; Temperature Controller\u003c\/span\u003e\u003c\/th\u003e \u003c\/tr\u003e \u003c\/thead\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd\u003eTemperature range\u003c\/td\u003e \u003ctd\u003e65...300 degC\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eTemperature stability\u003c\/td\u003e \u003ctd\u003e+\/-0,02 degC\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eTemperature control\u003c\/td\u003e \u003ctd\u003eTAC, self-optimizing (True Adaptive Control)\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eController\u003c\/td\u003e \u003ctd\u003ePilot ONE (E-grade \"Basic\")\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eSafety class\u003c\/td\u003e \u003ctd\u003eIII \/ FL\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eProtection class\u003c\/td\u003e \u003ctd\u003eIP20\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eDimensions (W x D x H)\u003c\/td\u003e \u003ctd\u003e425 x 250 x 631 mm | 16.73 x 9.84 x 24.84 inches\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eWeight\u003c\/td\u003e \u003ctd\u003e37 kg | 81.59 pounds\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd colspan=\"2\"\u003e\u003cspan\u003eHeating \/ Cooling Capacity\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eHeating capacity\u003c\/td\u003e \u003ctd\u003e4,8 kW\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd colspan=\"2\"\u003e\u003cspan\u003eCirculation Pump\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003ePressure pump max.\u003c\/td\u003e \u003ctd\u003e45 lpm ; 0.9 bar | 11.89 gpm ; 13.05 psi\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003ePump connection\u003c\/td\u003e \u003ctd\u003eM24x1,5 AG male\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003ePermissible viscosity\u003c\/td\u003e \u003ctd\u003e50 mm\/s\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd colspan=\"2\"\u003e\u003cspan\u003eConnections\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003ePt100 connection\u003c\/td\u003e \u003ctd\u003ePt100\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eAnalogue input\u003c\/td\u003e \u003ctd\u003evia optional Com.G@te\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eAnalogue output\u003c\/td\u003e \u003ctd\u003evia optional Com.G@te\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eDigital interface\u003c\/td\u003e \u003ctd\u003eRS232, Ethernet, USB Device, USB Host\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd colspan=\"2\"\u003e\u003cspan\u003eOperating Data\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eOld sku\u003c\/td\u003e \u003ctd\u003e1003.0022.01\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003ePermissible ambient temp.\u003c\/td\u003e \u003ctd\u003e5 to 40 degC\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eFilling volume min.\u003c\/td\u003e \u003ctd\u003e1.45 Liters | 0.38 gal\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eVolume of expansion\u003c\/td\u003e \u003ctd\u003e2.8 Liters | 0.74 gal\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003ePower supply\u003c\/td\u003e \u003ctd\u003e208V 3~ 60Hz\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eCurrent max.\u003c\/td\u003e \u003ctd\u003e15 A\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eFusing\u003c\/td\u003e \u003ctd\u003e15,5 A\u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e","brand":"BVV","offers":[{"title":"19 L Heater","offer_id":49567514755383,"sku":"50LGRDTK-19L","price":22500.0,"currency_code":"USD","in_stock":true},{"title":"Huber T305 Heater","offer_id":49567514788151,"sku":"50LGRDTK","price":52000.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/50l-turnkey-reactor-kit-300215.jpg?v=1726550000"},{"product_id":"20l-turnkey-reactor-kit","title":"BVV - 20L Turnkey Reactor Kit","description":"\u003ch2\u003e\u003cspan\u003e20L Turnkey Reactor Kit\u003c\/span\u003e\u003c\/h2\u003e \u003cp\u003eThe BVV 20L Double Jacketed Glass Reactor Kit is the ideal solution for small to medium-sized solvent recovery and decarboxylation applications. This kit includes everything to get you up and running including a Single 20L triple-layer Glass Reactor with Condenser, either a BVV 19L Heated circulator capable of heating to 220C or a UL-listed Huber CC-315B capable of heating up to 300C, a 1HP Polyscience 6160T for chilling the condenser, a Welch BTpro100 for vacuum, 25ft of 3\/8\" Gum rubber tubing for vacuum connections, 20ft of reinforced PVC hose for the chiller, 1\/2\" Stainless Steel JIC Hoses for the heater, 5 Gallons of Therminol Heat transfer fluid and 5 Gallons of Propylene glycol.\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cul\u003e\u003c\/ul\u003e \u003cp\u003e\u003cstrong\u003e20L Double Jacketed Glass Reactor Specifications\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003eGlass Material: GG-17 High Borosilicate Glass\u003c\/li\u003e \u003cli\u003eInternal Volume: 20L\u003cbr\u003e \u003c\/li\u003e \u003cli\u003e6.75L Jacket Capacity\u003c\/li\u003e \u003cli\u003eShelf Material: Aluminum Alloy\u003c\/li\u003e \u003cli\u003eHomogenizer Power: 110V\/60Hz\u003c\/li\u003e \u003cli\u003eHomogenizer Speed: 0-400 RPM\u003c\/li\u003e \u003cli\u003eDigital Homogenizer Control\u003c\/li\u003e \u003cli\u003eDigital temperature probe readout included\u003c\/li\u003e \u003cli\u003eDouble Jacket\u003c\/li\u003e \u003cli\u003e3\/4\" Jacket Connections\u003c\/li\u003e \u003cli\u003e1\/4\" and 3\/8\" Vacuum Connections\u003c\/li\u003e \u003cli\u003eLength: 20 in.\u003c\/li\u003e \u003cli\u003eWidth: 30 in.\u003c\/li\u003e \u003cli\u003eHeight: 76 in.\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003cstrong\u003ePolyscience 6100 1 HP Chiller Specifications\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003e6100 Series 1 HP Chiller with Turbine Pump, 100psi; 13.2l\/min\u003c\/li\u003e \u003cli\u003eDisplay: LED\u003c\/li\u003e \u003cli\u003eWorking Temperature Range C: -10 to 40\u003c\/li\u003e \u003cli\u003eTemperature Stability: +\/-0.1\u003c\/li\u003e \u003cli\u003eTemperature Calibration Capability: 1-point\u003c\/li\u003e \u003cli\u003ePump Type: Turbine\u003c\/li\u003e \u003cli\u003eWorking Temperature Range F: 14 to 104\u003c\/li\u003e \u003cli\u003eWorking Temperature Range C: -10 to 40\u003c\/li\u003e \u003cli\u003eReservoir Capacity (gallons): 1.11\u003c\/li\u003e \u003cli\u003eReservoir Capacity (liters): 4.2\u003c\/li\u003e \u003cli\u003eReservoir Cover: Screw-on cap\u003c\/li\u003e \u003cli\u003eCleanable Air Filter: Yes\u003c\/li\u003e \u003cli\u003eCleanable Fluid Filter: Yes\u003c\/li\u003e \u003cli\u003eTemperature Stability F: +\/-0.2\u003c\/li\u003e \u003cli\u003eTemperature Stability C: +\/-0.1\u003c\/li\u003e \u003cli\u003eDisplay: LED\u003c\/li\u003e \u003cli\u003eDisplay Resolution (Read): 0.1\u003c\/li\u003e \u003cli\u003ePump Type: Turbine\u003c\/li\u003e \u003cli\u003eProcess Connections: 1\/2\" FNPT\u003c\/li\u003e \u003cli\u003eOver-Temperature Protection \/ Failsafe Heater Control: Yes\u003c\/li\u003e \u003cli\u003eReservoir Liquid Level Indicator: Yes\u003c\/li\u003e \u003cli\u003eReservoir Drain: Yes\u003c\/li\u003e \u003cli\u003eCool Command Refrigeration Technology: Yes\u003c\/li\u003e \u003cli\u003eWhisperCool Environmental Control Technology: Yes\u003c\/li\u003e \u003cli\u003eMaximum Ambient Temperature F: 95\u003c\/li\u003e \u003cli\u003eMaximum Ambient Temperature C: 35\u003c\/li\u003e \u003cli\u003eOverall Dimensions (LxWxH inches): 27.6 x 14.5 x 22.6\u003c\/li\u003e \u003cli\u003eOverall Dimensions (LxWxH cm): 70 x 36.8 x 57.5\u003c\/li\u003e \u003cli\u003eCompressor Size (HP): 1\u003c\/li\u003e \u003cli\u003eRefrigerant: R134a\u003c\/li\u003e \u003cli\u003eShipping Weight (pounds): 199\u003c\/li\u003e \u003cli\u003eShipping Weight (kilograms): 90\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003cstrong\u003eWelch BTpro100 Specifications\u003c\/strong\u003e\u003c\/p\u003e \u003ctable\u003e \u003cthead\u003e \u003ctr\u003e \u003cth\u003eModel\u003c\/th\u003e \u003cth\u003eBTpro100\u003c\/th\u003e \u003c\/tr\u003e \u003c\/thead\u003e \u003ccolgroup\u003e \u003ccol\u003e \u003ccol\u003e \u003c\/colgroup\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd\u003eFree Air Displacement@60Hz,\u003cbr\u003elpm(CFM)\u003c\/td\u003e \u003ctd\u003e100(3.5)\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eUltimate Vacuum Pressure, Torr\u003c\/td\u003e \u003ctd\u003e6\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eMaximum Vacuum, in. Hg\u003c\/td\u003e \u003ctd\u003e29.7\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eHorsepower, HP (watts)\u003c\/td\u003e \u003ctd\u003e0.5(390)\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eBuilt-in adjustable vacuum\u003c\/td\u003e \u003ctd\u003e-\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eGas Ballast\u003c\/td\u003e \u003ctd\u003eYes\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eHead Material\u003c\/td\u003e \u003ctd\u003ePTFE\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eDiaphragm\u003c\/td\u003e \u003ctd\u003ePTFE\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eInlet\/outlet Connection\u003c\/td\u003e \u003ctd\u003e \u003cp\u003eNW16 flange\u003csup\u003e1\u003c\/sup\u003e\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eAgency (National Recognized Lab)\u003c\/td\u003e \u003ctd\u003ecUL\u003cbr\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eWeight, lbs (kg)\u003c\/td\u003e \u003ctd\u003e40.3(18.3)\u003cbr\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eOverall Dimensions\u003cbr\u003e\u003cbr\u003e\u003cbr\u003eLxWxH in.(cm)\u003c\/td\u003e \u003ctd\u003e9x15x7\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e(23x38x18)\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eShipping Weight, lbs(kg)\u003c\/td\u003e \u003ctd\u003e48.5 (22)\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eShipping Carton Dimensions\u003cbr\u003e\u003cbr\u003e\u003cbr\u003eLxWxH in.(cm)\u003c\/td\u003e \u003ctd\u003e18.9x12.6x11.8\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e(48x32x30)\u003cbr\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003cstrong\u003eHUBER CC-315B Specifications\u003c\/strong\u003e\u003c\/p\u003e \u003ctable\u003e \u003cthead\u003e \u003ctr\u003e \u003cth colspan=\"2\"\u003e\u003cspan\u003eCommon Specifications\u003c\/span\u003e\u003c\/th\u003e \u003c\/tr\u003e \u003c\/thead\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd\u003eTemperature range\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003e(-20) 28...300 degC\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eTemperature stability\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003e+\/-0.02 degC\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eTemperature control\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003eTAC, self-optimizing (True Adaptive Control)\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eController\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003ePilot ONE (E-grade \"basic\")\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eSafety class\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003eIII \/ FL\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eProtection class\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003eIP20\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eDimensions (W x D x H)\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003e13.19 x 15.04 x 17.05 inches\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eWeight\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003e48.51 pounds\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd colspan=\"2\"\u003e\u003cspan\u003eHeating \/ cooling capacity\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eHeating capacity\u003c\/td\u003e \u003ctd\u003e3 - 3,5 kW\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd colspan=\"2\"\u003e\u003cspan\u003eCirculation pump\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003ePressure pump max.\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003e25 lpm : 0,7 bar | 6.6 gpm ; 10.15 psi\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eSuction pump max.\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003e18.5 lpm : 0,4 bar | bar 4.89 gpm ; 5.8 psi\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003ePump connection\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003eM16x1 AG male\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003ePermissible viscosity\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003e50 mm\/s\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd colspan=\"2\"\u003e\u003cspan\u003eConnections\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003ePt100 connection\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003ePt100\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eDigital interface\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003eRS232, Ethernet, USB Device, USB Host\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd colspan=\"2\"\u003e\u003cspan\u003eOperating data\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eOld sku\u003c\/td\u003e \u003ctd\u003e2007.0003.01\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003ePermissible ambient temp.\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003e5...40 degC\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eBath opening W x D \/ BD\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003e10.63 x 5.71 \/ 7.87 inches\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eBath volume\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003e15 Liters | 3.96 gal\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eFilling volume min.\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003e11.5 Liters | 3.04 gal\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003ePower supply\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003e208V 2~ 60Hz\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eCurrent max.\u003c\/td\u003e \u003ctd\u003e\u003cspan\u003e16 A\u003c\/span\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eFusing\u003c\/td\u003e \u003ctd\u003e20 A\u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e","brand":"BVV","offers":[{"title":"19 L Heater","offer_id":49567515476279,"sku":"20LGRDTK-19L","price":21000.0,"currency_code":"USD","in_stock":true},{"title":"Huber CC-315 Heater","offer_id":49567515509047,"sku":"20LGRDTK","price":31000.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/20l-turnkey-reactor-kit-918649.jpg?v=1726549813"},{"product_id":"bvv-6-falling-film-evaporator","title":"BVV - 6 in Falling Film Evaporator","description":"\u003cul\u003e \u003cli\u003e\u003ca href=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/CutSheet_BVV-20GPH_FallingFilmEvaporator_1.pdf?v=1639769496\" title=\"Falling Film Cutsheet\" target=\"_blank\"\u003e\u003cstrong\u003eBVV 6\" Falling Film Evaporator Cutsheet\u003c\/strong\u003e\u003c\/a\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003eIs your lab floor filled with a fleet of rotary evaporators? Looking to increase solvent recovery throughput? Our new and compact 20GPH Falling Film Evaporator (FFE) has the capability to maximize throughput and replace up to five 50L Rotary Evaporators.\u003c\/p\u003e \u003cp\u003eThe BVV 20GPH Falling Film Evaporator is designed to evaporate ethanol that has been diluted in crude oil during a filtration or extraction process. By reducing the vapor pressure inside the system and metering the injection valve, the user can set the heat exchangers to the appropriate temperatures to efficiently evaporate solvent from their crude oil.\u003c\/p\u003e \u003cp\u003eWe paired our FFE with reliable equipment that will keep operations running. End users are required to plumb the process inlet and outlet connections for both heat exchangers. They are supplied with 1.5\" sanitary tri-clamp connections. BVV can assist with necessary parts needed for a permanent or temporary installation. Temporary installations may be necessary if your lab has limited fume hoods or space which is shared with other processing equipment.\u003c\/p\u003e \u003cp\u003eBelow you will find key features, additional equipment included with the system and the power requirements for each, and real-life efficiencies that were tested.\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eKey Features: \u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e* Compact rack design for use in fume hoods (39\"x30\"x75.5\")\u003c\/p\u003e \u003cp\u003e* Vernier scale metering valve for controlled injection\u003c\/p\u003e \u003cp\u003e* Accurate heater and chiller temperature control\u003c\/p\u003e \u003cp\u003e* Deep vacuum for effective solvent removal\u003c\/p\u003e \u003cp\u003e* Discharge pumps to eliminate constant reservoir draining and down time\u003c\/p\u003e \u003cp\u003e* Chemical resistant vacuum pump\u003c\/p\u003e \u003cp\u003e* Adaptable discharge outlets to customer preference\u003c\/p\u003e \u003cp\u003e* Insulation to limit thermal loses and reduce condensation (Not Pictured)\u003c\/p\u003e \u003cp\u003e* Sanitary tri-clamp and compression fittings\u003c\/p\u003e \u003cp\u003e* Pre-heat injection coil\u003c\/p\u003e \u003cp\u003e* Injection distribution plate\u003c\/p\u003e \u003cp\u003e* Tube in shell heat exchanger for efficient evaporation and condensation\u003c\/p\u003e \u003cp\u003e* Packable vapor path for reduction of contaminants and cleaner separation\u003c\/p\u003e \u003cp\u003e* Water reservoir for priming the heating system and expansion during operation\u003c\/p\u003e \u003ctable cellpadding=\"0\" cellspacing=\"0\" border=\"0\"\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd valign=\"top\"\u003e \u003cdiv\u003e\u003cimg src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/products\/FFE-6X36-01-11_240x240.jpg?v=1639434191\" alt=\"\"\u003e\u003c\/div\u003e \u003c\/td\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003eCrude Discharge Pump\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003eEasily control discharge speed and collect your extract directly from the 3\/8\" tube via a collection vessel or swage on a fitting of your preference to pump collected extract to a secondary location. Eliminate constant reservoir draining and operate continuously.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cimg src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/products\/FFE-6X36-01-2_240x240.jpg?v=1639434201\" alt=\"\"\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003eMetered Solvent Injection\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003eEffectively repeat efficiency and throughput with our vernier scale metering valve. Easy to dial in the desired efficiency and throughput desired by the user.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cimg src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/products\/FFE-6X36-01-3_240x240.jpg?v=1639434154\" alt=\"\"\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003eDistribution Plate\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003eDirects the injected solvent to be evenly distributed across all tubes in the heat exchanger which maximizes the effective heating surface area.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cimg src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/products\/FFE-6X36-01-4_240x240.jpg?v=1639434273\" alt=\"\"\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003eSolvent Discharge and Vacuum Pump\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003eThe solvent discharge pump eliminates the need for a reservoir and allows you to pump recovered solvent to any desired secondary location.\u003c\/p\u003e \u003cp\u003eThe vacuum pump manifold gives you easy vacuum control during the complete operation.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003cstrong\u003ePOWER REQUIREMENTS\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003eThe equipment listed below is included with the system. Check power requirements and amp draw prior to purchasing.\u003c\/p\u003e \u003ctable width=\"639\" cellpadding=\"0\" cellspacing=\"0\" border=\"0\"\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd valign=\"top\" width=\"208\"\u003e \u003cp\u003e\u003cstrong\u003eEquipment \u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"132\"\u003e \u003cp\u003e\u003cstrong\u003ePurpose\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"104\"\u003e \u003cp\u003e\u003cstrong\u003ePower Requirement\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"81\"\u003e \u003cp align=\"center\"\u003e\u003cstrong\u003eAmp Draw\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"114\"\u003e \u003cp\u003e\u003cstrong\u003eNotes\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd valign=\"top\" width=\"208\"\u003e \u003cp\u003e2GPM Ethanol Recovery Pump for Vacuum\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"132\"\u003e \u003cp\u003ePump for Ethanol Recovery Discharge\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"104\"\u003e \u003cp\u003e230V 1-Phase\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"81\"\u003e \u003cp align=\"center\"\u003e2.4\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"114\"\u003e \u003cp\u003e2GPM Max Flow Rate, Vacuum Check Valve\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd valign=\"top\" width=\"208\"\u003e \u003cp\u003eBeaker and Wrench Explosion Proof Oil Pump\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"132\"\u003e \u003cp\u003ePump for Oil Recovery Discharge\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"104\"\u003e \u003cp\u003e230V 1-Phase\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"81\"\u003e \u003cp align=\"center\"\u003e1.1\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"114\"\u003e \u003cp\u003e90L\/hr. Max Flow Rate, Vacuum Check Valve\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd valign=\"top\" width=\"208\"\u003e \u003cp\u003eWelch BTpro100 Diaphragm Pump\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"132\"\u003e \u003cp\u003eVacuum Pump for System\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"104\"\u003e \u003cp\u003e115 1-Phase\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"81\"\u003e \u003cp align=\"center\"\u003e3.4\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"114\"\u003e \u003cp\u003e3.5 CFM, 6 Torr Ultimate Vacuum\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd valign=\"bottom\" colspan=\"2\" width=\"340\"\u003e\u003c\/td\u003e \u003ctd valign=\"top\" width=\"104\"\u003e \u003cp align=\"center\"\u003e\u003cstrong\u003eTotal Amp Draw\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"81\"\u003e \u003cp align=\"center\"\u003e\u003cstrong\u003e6.9\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"bottom\" width=\"114\"\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eEFFICIENCY\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003eWe are proud to present real data with running parameters and efficiencies that reflect the actual operation of our system. Below you will find the tested throughputs and efficiencies that our FFE is capable of handling.\u003c\/p\u003e \u003ctable width=\"641\" cellpadding=\"0\" cellspacing=\"0\" border=\"1\"\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd valign=\"top\" width=\"107\"\u003e \u003cp\u003e\u003cstrong\u003eThroughput\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"107\"\u003e \u003cp\u003e11 GPH\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"107\"\u003e \u003cp\u003e18 GPH\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"107\"\u003e \u003cp\u003e20 GPH\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"107\"\u003e \u003cp\u003e22 GPH\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"107\"\u003e \u003cp\u003e24 GPH\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd valign=\"top\" width=\"107\"\u003e \u003cp\u003e\u003cstrong\u003eEfficiency \u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"107\"\u003e \u003cp\u003e98%\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"107\"\u003e \u003cp\u003e97%\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"107\"\u003e \u003cp\u003e94%\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"107\"\u003e \u003cp\u003e90%\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\" width=\"107\"\u003e \u003cp\u003e85%\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cp\u003e** Efficiency calculated at 10:1 ratio (Ethanol : Crude Oil) with heater temperature of 160degF. Crude is fully dewaxed when going into the falling film evaporator. Solution starts at room temperature. Speeds may differ based on dilution ratio, crude quality, and running parameters. ** \u003cstrong\u003e\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567535563063,"sku":"FFE-6X36","price":64400.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/2eb343d01beaf24a12eb0c21adb93075.jpg?v=1758127152"},{"product_id":"bvv-6-turnkey-falling-film-evaporator","title":"BVV - 6 in Turnkey Falling Film Evaporator","description":"\u003cul\u003e \u003cli\u003e\u003ca title=\"Falling Film Cutsheet\" href=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/CutSheet_BVV-20GPH_FallingFilmEvaporator_1.pdf?v=1639769496\" target=\"_blank\"\u003e\u003cstrong\u003eBVV 6\" Turnkey Falling Film Evaporator Cutsheet\u003c\/strong\u003e\u003c\/a\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003eIs your lab floor filled with a fleet of rotary evaporators? Looking to increase solvent recovery throughput? Our new and compact 20GPH Falling Film Evaporator (FFE) has the capability to maximize throughput and replace up to five 50L Rotary Evaporators.\u003c\/p\u003e \u003cp\u003eThe BVV 20GPH Falling Film Evaporator is designed to evaporate ethanol that has been diluted in crude oil during a filtration or extraction process. By reducing the vapor pressure inside the system and metering the injection valve, the user can set the heat exchangers to the appropriate temperatures to efficiently evaporate solvent from their crude oil.\u003c\/p\u003e \u003cp\u003eWe paired our FFE with reliable equipment that will keep operations running. End users are required to plumb the process inlet and outlet connections for both heat exchangers. They are supplied with 1.5\" sanitary tri-clamp connections. BVV can assist with necessary parts needed for a permanent or temporary installation. Temporary installations may be necessary if your lab has limited fume hoods or space which is shared with other processing equipment.\u003c\/p\u003e \u003cp\u003eBelow you will find key features, additional equipment included with the system and the power requirements for each, and real-life efficiencies that were tested.\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eKey Features: \u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e* Compact rack design for use in fume hoods (39\"x30\"x75.5\")\u003c\/p\u003e \u003cp\u003e* Vernier scale metering valve for controlled injection\u003c\/p\u003e \u003cp\u003e* Accurate heater and chiller temperature control\u003c\/p\u003e \u003cp\u003e* Deep vacuum for effective solvent removal\u003c\/p\u003e \u003cp\u003e* Discharge pumps to eliminate constant reservoir draining and down time\u003c\/p\u003e \u003cp\u003e* Chemical resistant vacuum pump\u003c\/p\u003e \u003cp\u003e* Adaptable discharge outlets to customer preference\u003c\/p\u003e \u003cp\u003e* Insulation to limit thermal loses and reduce condensation (Not Pictured)\u003c\/p\u003e \u003cp\u003e* Sanitary tri-clamp and compression fittings\u003c\/p\u003e \u003cp\u003e* Pre-heat injection coil\u003c\/p\u003e \u003cp\u003e* Injection distribution plate\u003c\/p\u003e \u003cp\u003e* Tube in shell heat exchanger for efficient evaporation and condensation\u003c\/p\u003e \u003cp\u003e* Packable vapor path for reduction of contaminants and cleaner separation\u003c\/p\u003e \u003cp\u003e* Water reservoir for priming the heating system and expansion during operation\u003c\/p\u003e \u003cp\u003e\u003cspan\u003e* The certified model is 22 State certified by PRV Engineers and includes an Infield Verification by PRV Engineers within the purchase price. States include but are not limited to: Alabama, Arizona, Arkansas, California, Colorado, Connecticut, Florida, Illinois, Kansas, Louisiana, Maine, Massachusetts, Missouri, Nevada, North Carolina, Oklahoma, Oregon, Texas, Vermont, Washington, West Virginia, and Wyoming\u003c\/span\u003e\u003c\/p\u003e \u003ctable border=\"0\" cellspacing=\"0\" cellpadding=\"0\"\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd valign=\"top\"\u003e \u003cdiv\u003e\u003cimg alt=\"\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/products\/FFE-6X36-01-11_240x240.jpg?v=1639434191\"\u003e\u003c\/div\u003e \u003c\/td\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003eCrude Discharge Pump\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003eEasily control discharge speed and collect your extract directly from the 3\/8\" tube via a collection vessel or swage on a fitting of your preference to pump collected extract to a secondary location. Eliminate constant reservoir draining and operate continuously.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cimg alt=\"\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/products\/FFE-6X36-01-2_240x240.jpg?v=1639434201\"\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003eMetered Solvent Injection\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003eEffectively repeat efficiency and throughput with our vernier scale metering valve. Easy to dial in the desired efficiency and throughput desired by the user.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cimg alt=\"\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/products\/FFE-6X36-01-3_240x240.jpg?v=1639434154\"\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003eDistribution Plate\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003eDirects the injected solvent to be evenly distributed across all tubes in the heat exchanger which maximizes the effective heating surface area.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cimg alt=\"\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/products\/FFE-6X36-01-4_240x240.jpg?v=1639434273\"\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003eSolvent Discharge and Vacuum Pump\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003eThe solvent discharge pump eliminates the need for a reservoir and allows you to pump recovered solvent to any desired secondary location.\u003c\/p\u003e \u003cp\u003eThe vacuum pump manifold gives you easy vacuum control during the complete operation.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003cstrong\u003ePOWER REQUIREMENTS\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003eThe equipment listed below is included with the system. Check power requirements and amp draw prior to purchasing.\u003c\/p\u003e \u003ctable border=\"0\" cellspacing=\"0\" cellpadding=\"0\" width=\"639\"\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd width=\"208\" valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003eEquipment \u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"132\" valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003ePurpose\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"104\" valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003ePower Requirement\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"81\"\u003e \u003cp align=\"center\"\u003e\u003cstrong\u003eAmp Draw\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"114\" valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003eNotes\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd width=\"208\" valign=\"top\"\u003e \u003cp\u003eHubbell Process Water Heater\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"132\"\u003e \u003cp\u003eHeater for Heat Exchanger Column (Evaporation)\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"104\"\u003e \u003cp\u003e240V 3-Phase\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"81\"\u003e \u003cp align=\"center\"\u003e87\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"114\" valign=\"top\"\u003e \u003cp\u003e36kW Heating Capacity\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd width=\"208\" valign=\"top\"\u003e \u003cp\u003eTaco ECM High-Efficiency Circulator\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"132\"\u003e \u003cp\u003eWater Circulator for Heater\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"104\"\u003e \u003cp\u003e115V 1-Phase\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"81\"\u003e \u003cp align=\"center\"\u003e2.5\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"114\" valign=\"top\"\u003e \u003cp\u003eMax flow rate 52GPM\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd width=\"208\" valign=\"top\"\u003e \u003cp\u003e10hp Polyscience Chiller 230v\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"132\"\u003e \u003cp\u003eChiller for Heat Exchanger Column (Condensation)\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"104\"\u003e \u003cp\u003e230V 3-Phase\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"81\"\u003e \u003cp align=\"center\"\u003e78\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"114\" valign=\"top\"\u003e \u003cp\u003e38.7kW Cooling Capacity\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd width=\"208\" valign=\"top\"\u003e \u003cp\u003e2GPM Ethanol Recovery Pump for Vacuum\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"132\"\u003e \u003cp\u003ePump for Ethanol Recovery Discharge\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"104\"\u003e \u003cp\u003e230V 1-Phase\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"81\"\u003e \u003cp align=\"center\"\u003e2.4\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"114\" valign=\"top\"\u003e \u003cp\u003e2GPM Max Flow Rate, Vacuum Check Valve\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd width=\"208\" valign=\"top\"\u003e \u003cp\u003eBeaker and Wrench Explosion Proof Oil Pump\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"132\"\u003e \u003cp\u003ePump for Oil Recovery Discharge\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"104\"\u003e \u003cp\u003e230V 1-Phase\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"81\"\u003e \u003cp align=\"center\"\u003e1.1\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"114\" valign=\"top\"\u003e \u003cp\u003e90L\/hr. Max Flow Rate, Vacuum Check Valve\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd width=\"208\" valign=\"top\"\u003e \u003cp\u003eWelch BTpro100 Diaphragm Pump\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"132\"\u003e \u003cp\u003eVacuum Pump for System\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"104\"\u003e \u003cp\u003e115 1-Phase\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"81\"\u003e \u003cp align=\"center\"\u003e3.4\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"114\" valign=\"top\"\u003e \u003cp\u003e3.5 CFM, 6 Torr Ultimate Vacuum\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd width=\"340\" colspan=\"2\" valign=\"bottom\"\u003e\u003c\/td\u003e \u003ctd width=\"104\" valign=\"top\"\u003e \u003cp align=\"center\"\u003e\u003cstrong\u003eTotal Amp Draw\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"81\" valign=\"top\"\u003e \u003cp align=\"center\"\u003e\u003cstrong\u003e174.4\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"114\" valign=\"bottom\"\u003e\u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eEFFICIENCY\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003eWe are proud to present real data with running parameters and efficiencies that reflect the actual operation of our system. Below you will find the tested throughputs and efficiencies that our FFE is capable of handling.\u003c\/p\u003e \u003ctable border=\"1\" cellspacing=\"0\" cellpadding=\"0\" width=\"641\"\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd width=\"107\" valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003eThroughput\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"107\" valign=\"top\"\u003e \u003cp\u003e11 GPH\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"107\" valign=\"top\"\u003e \u003cp\u003e18 GPH\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"107\" valign=\"top\"\u003e \u003cp\u003e20 GPH\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"107\" valign=\"top\"\u003e \u003cp\u003e22 GPH\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"107\" valign=\"top\"\u003e \u003cp\u003e24 GPH\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd width=\"107\" valign=\"top\"\u003e \u003cp\u003e\u003cstrong\u003eEfficiency \u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"107\" valign=\"top\"\u003e \u003cp\u003e98%\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"107\" valign=\"top\"\u003e \u003cp\u003e97%\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"107\" valign=\"top\"\u003e \u003cp\u003e94%\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"107\" valign=\"top\"\u003e \u003cp\u003e90%\u003c\/p\u003e \u003c\/td\u003e \u003ctd width=\"107\" valign=\"top\"\u003e \u003cp\u003e85%\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cp\u003e** Efficiency calculated at 10:1 ratio (Ethanol : Crude Oil) with heater temperature of 160degF. Crude is fully dewaxed when going into the falling film evaporator. Solution starts at room temperature. Speeds may differ based on dilution ratio, crude quality, and running parameters. ** \u003cstrong\u003e\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e","brand":"BVV","offers":[{"title":"Non-Certified","offer_id":49567578358071,"sku":"FFE-6X36-01","price":129600.0,"currency_code":"USD","in_stock":true},{"title":"Certified","offer_id":49567578390839,"sku":"FFE-6X36-01-CERT","price":135360.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/38d11454a61779c183120b3a54c771af.jpg?v=1758127245"},{"product_id":"2l-full-bore-short-path-distillation-turnkey-kit-with-p2-distillation-head","title":"BVV - 2L Full Bore Short Path Distillation Turnkey Kit with P2 Distillation Head","description":"\u003cp\u003e \u003c\/p\u003e \u003ch2\u003e2L Full Bore Short Path Distillation Turnkey Kit with P2 Distillation Head\u003c\/h2\u003e \u003ch6\u003e\u003cem\u003e\u003cu\u003eThis unit carries a 2-day lead time\u003c\/u\u003e\u003c\/em\u003e\u003c\/h6\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003eThe 2L Full Bore Short Path Distillation Turnkey Kit with P2 Distillation Head is a great setup for smaller scale processors that want a budget friendly system without sacrificing quality on the main components that make a short path great. We understand that as an operator our customers want to be able to start their system and operate in ideal conditions run after run. That is why we paired a full-bore setup with a 14.1CFM pump that will assure the lowest vacuum depth will be pulled every time. Main components such as the distillation head, vacuum valve adapter, and cold trap are all American blown glass. These components allow us to present this system that will repeat in performance time after time. \u003c\/p\u003e \u003cp\u003eFor a in depth analysis of this system please view the following videos. Here you will see the system setup, component explanation, and even see it perform in a first and second distillation pass. These runs were all performed in our lab and the data was used to help fine tune the system.\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003ca href=\"https:\/\/www.youtube.com\/watch?v=6nUYPty2luU\" target=\"_blank\"\u003e\u003cstrong\u003eVideo 1 - Setup and Component Explanation\u003c\/strong\u003e\u003c\/a\u003e\u003c\/p\u003e \u003cp\u003e\u003ca href=\"https:\/\/www.youtube.com\/watch?v=6nUYPty2luU\" target=\"_blank\"\u003e\u003cstrong\u003e\u003cimg alt=\"\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/video_1_480x480.png?v=1625852603\"\u003e\u003c\/strong\u003e\u003c\/a\u003e\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003ca href=\"https:\/\/www.youtube.com\/watch?v=vezZHQc02TI\" target=\"_blank\"\u003e\u003cstrong\u003eVideo 2 - Setup Addendum\u003c\/strong\u003e\u003c\/a\u003e\u003c\/p\u003e \u003cp\u003e\u003ca href=\"https:\/\/www.youtube.com\/watch?v=vezZHQc02TI\" target=\"_blank\"\u003e\u003cstrong\u003e\u003cimg alt=\"\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/video_2_84cb653b-c33d-4a14-809c-0139a48c042e_480x480.png?v=1625853010\"\u003e\u003c\/strong\u003e\u003c\/a\u003e\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003ca href=\"https:\/\/www.youtube.com\/watch?v=N_XOiFQJi7I\" target=\"_blank\"\u003e\u003cb\u003eVideo 3 - Fist pass Distillation\u003c\/b\u003e\u003c\/a\u003e\u003c\/p\u003e \u003cp\u003e\u003ca href=\"https:\/\/www.youtube.com\/watch?v=N_XOiFQJi7I\" target=\"_blank\"\u003e\u003cb\u003e\u003cimg alt=\"\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/video_3_9a53d6ce-5518-477e-b3df-5135897ba8f0_480x480.png?v=1625853111\"\u003e\u003c\/b\u003e\u003c\/a\u003e\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003ca href=\"https:\/\/www.youtube.com\/watch?v=vqbFLwHa-9c\" target=\"_blank\"\u003e\u003cb\u003e\u003cstrong\u003eVideo 4 - Second Pass Distillation\u003c\/strong\u003e\u003c\/b\u003e\u003c\/a\u003e\u003c\/p\u003e \u003cp\u003e\u003ca href=\"https:\/\/www.youtube.com\/watch?v=vqbFLwHa-9c\" target=\"_blank\"\u003e\u003cb\u003e\u003cstrong\u003e\u003cimg alt=\"\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/video_4_480x480.png?v=1625853154\"\u003e\u003c\/strong\u003e\u003c\/b\u003e\u003c\/a\u003e\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003ctable\u003e \u003ccolgroup\u003e \u003ccol\u003e \u003ccol\u003e \u003c\/colgroup\u003e \u003cthead\u003e \u003ctr\u003e \u003cth colspan=\"2\"\u003eThe 2L Full Bore Short Path Distillation Turnkey Kit with P2 Distillation Head Includes:\u003c\/th\u003e \u003c\/tr\u003e \u003c\/thead\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003eFirst Pass Distillation Operating Procedure\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003eP2 Distillation Kit\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003e2L Double Neck Boiling Flask\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003eFull Bore Vacuum Valve Adapter\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003eBVV MP7H Heater\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003e2L Heating Mantle\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003eRibbed Glass Cold Trap\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003eBullseye Precision Vacuum Gauge\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003eBVV Pro Series 14.1CFM Rotary Vane Pump (Comes filled with oil. Recommend purchasing additional Ultra 19 Vacuum Pump Oil. SKU: INLAND19-ULTRS-1G)\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003eOil Mist Filter Trap for Rotary Vane Pump\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003e24\/40 250ml Single Neck Round Bottom Flask\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e3\u003c\/td\u003e \u003ctd\u003e24\/40 500ml Single Neck Round Bottom Flask\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003e24\/40 Glass Funnel\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003eVacuum Manifold for Rotary Vane Pump\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003e1 Meter Bellow Hose\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003ePTFE Magnetic Stirring Bar Retriever\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003e24\/40 Metal Keck Clip\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e6\u003c\/td\u003e \u003ctd\u003e24\/40 Plastic Keck Clips\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e3\u003c\/td\u003e \u003ctd\u003e250-500ml Cork Stands\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e2\u003c\/td\u003e \u003ctd\u003eChain Clamps\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003eBoss Head with 3 Finger Clamp\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003eBVV Lab Stand\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e10\u003c\/td\u003e \u003ctd\u003eFiber Glass Insulation Rope\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003eDow Corning High Vacuum Grease\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003e10\/30 Non-Mercury Glass Thermometers\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003e24\/40 - 10\/30 Glass Adapter Bushing\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003e24\/40 - 1\/8\" Thermometer Adapter\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e1\u003c\/td\u003e \u003ctd\u003e24\/40 Straight Adapter\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e2\u003c\/td\u003e \u003ctd\u003e6\"x6\" Scissor Jack\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e3\u003c\/td\u003e \u003ctd\u003e36\" Threaded Lab Stand Rod\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e2\u003c\/td\u003e \u003ctd\u003eGl14 - 8mm Barb\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e6\u003c\/td\u003e \u003ctd\u003e1\/4\" Silicone Tubing\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e2\u003c\/td\u003e \u003ctd\u003ePTFE Magnetic Stirring Bar\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e4\u003c\/td\u003e \u003ctd\u003eHose Clamp with Butterfly Key\u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Note: This entire setup will ship via motor freight.***\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567589105975,"sku":"2LFBTK-14.1","price":7500.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/f8aa01109f91c70cced270d4c6b013b9.jpg?v=1758128187"},{"product_id":"5l-neocision-etl-lab-certified-rotary-evaporator-turnkey-system","title":"BVV - 5L Neocision ETL Lab Certified Rotary Evaporator Turnkey System","description":"\u003ch2\u003e5L Neocision ETL Lab Certified Rotary Evaporator Turnkey System\u003c\/h2\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003eThe 5L Neocision ETL Lab Certified Rotary Evaporator is a full-scale system meant to fulfill the needs of large volume production and meet the requirements of a certified laboratory with its ETL certification standards. Featuring an electric lift bath and all PTFE valves for extreme chemical resistance, the 5L Neocision gives users the ability to recover large amounts of solvent in a smaller footprint with highly improved functionality. All Neocision rotovaps feature high-efficiency valves and drain ports making it easy to directly inject solution continuously without the need to stop the system or release vacuum to drain. The temperature and rotation speed are easily controlled from a single digital interface. Our rotovaps are a fraction of the price of more costly systems with the same functionality and evaporation efficiency. \u003c\/span\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003e\u003cimg width=\"900\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_rotovapflowchart_jpg?18265071413647998907\" alt=\"Rotovap Flow Chart\" title=\"Rotovap Flow Chart\"\u003e\u003c\/span\u003e\u003c\/p\u003e \u003ch3\u003e\u003cbr\u003e\u003c\/h3\u003e \u003cp\u003e\u003cstrong\u003e5L NEO Rotary Evaporator Turnkey System setup includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003e5L Neocision ETL Lab Certified Rotary Evaporator\u003cbr\u003e \u003c\/li\u003e \u003cli\u003e\u003ca href=\"https:\/\/shopbvv.com\/products\/polyscience-ls-20c-to-40c-1-2hp-chiller-w-turbine-pump\" title=\"Polysciences LS20\" rel=\"noopener noreferrer\" target=\"_blank\"\u003ePolyscience LS -20C to 40C 1\/2HP Chiller w\/ Turbine Pump\u003c\/a\u003e\u003c\/li\u003e \u003cli\u003e1\/4\" Gum Rubber - 100ft\u003cbr\u003e \u003c\/li\u003e \u003cli\u003e1\/4\" Silicone Tubing - 25ft\u003c\/li\u003e \u003cli\u003e\u003ca title=\"Welch BTPRO 70\" href=\"https:\/\/shopbvv.com\/products\/welch-btpro70\" target=\"_blank\"\u003eWelch BTpro70\u003c\/a\u003e\u003c\/li\u003e \u003cli\u003eAdjustable Stainless Steel Hose Clamps\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eFeatures:\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eETL Certified for Lab use.\u003c\/li\u003e \u003cli\u003eDigital temperature and speed control with simple user interface\u003c\/li\u003e \u003cli\u003eElectric Bath Lift\u003c\/li\u003e \u003cli\u003eTeflon Coated Bath for corrosion resistance\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eHigh-efficiency drain port and injection valves\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eSmaller footprint for improved workspace allocation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eMobility with locking casters\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eShorter vapor path for faster evaporation and condensation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDirect injection capability for continuous feeding of solution\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eContinuous draining capability without the need to release vacuum or stop the system\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1-year warranty on all mechanical parts. \u003cem\u003eDoes not include glassware. \u003c\/em\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSpecifications:\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003ctable height=\"1537\" border=\"1\"\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eModel\u003c\/b\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003e5L Solvent Pro Series Rotary Evaporator \u003c\/b\u003e\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eOptimum Ambient Temperature\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e5~25C \/ 41~105.8F\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eGlass Material\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eGG-17 High Borosilicate\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003ePower (V\/Hz)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e110V 50\/60Hz Single Phase\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eSpeed Regulation\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eDigital Step-less Regulation\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eRotation Speed\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e20-130 RPM\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eSet Temperature\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eRT+5 - 99C\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eTemperature Control\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eDigital Temperature Control\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eMaximum Vacuum Pressure\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e-29.8 inHg\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eEvaporating Flask Capacity\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e5L (5000ml)\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eReceiving Flask Capacity\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e5L (5000ml)\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eCondenser Style\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eMain + Auxiliary Vertical Double Helix\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eHeater Max Current Draw (Amps)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e25\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWater Bath Material\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e304 Stainless Steel\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWater Bath Size\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e17.7 x 9.8 in.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eLifting Function\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eElectric\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eLifting Stroke\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e190mm \/ 7.5 in.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eTotal Power Consumption (kW)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e1800w\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eDimensions\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e45 x 32 x 15in\u003cbr\u003e\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWeight\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e155 lbs\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eVacuum Connection\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e14mm \/ .55 in. Barb\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eCondenser Connection\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e18mm \/ .70 in. Barb\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWarranty\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e1 Year excluding glass parts\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eCertifications\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eETL\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eRotovap Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for rotovaps. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs. \u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eClean and assemble unit. Make sure all pieces are cleaned and sterilized using an alcohol solution.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect chiller to condenser and set to 0C (32F). Always fill a rotovap condenser from the top down (chiller output to top of condenser, chiller input to bottom of condenser).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect vacuum pump to cold trap and connect cold trap to vacuum port on rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTurn on heat bath and set to 40C (113F).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce heat bath, chiller and cold trap have reached desired temperatures, turn on rotovap motor and set speed to approximately 100 RPM (does not have to be precise). Keep in mind, higher RPM's will increase evaporation power but also increase heat load.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eStart vacuum pump and allow vacuum to pull down for a few minutes before injection.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce vacuum has been pulled to a sufficient level (does not have to be precise but should be below 100 Torr), using the injection valve, very slowly inject approximately 500 mL of solution into evaporating flask and then close the valve. Allow this small amount to begin evaporating. You may see the chiller begin to rise in temperature, this is called \"priming\" the rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce the temperature stops rising or all liquid is almost completely evaporated, open the injection valve again very slowly so that a small amount of liquid begins to enter the evaporating flask. Do not close injection valve this time but continue to allow solution to enter the evaporating flask.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAt this point you must try to match the input speed to the output speed. What this means is that you should be injecting the same amount of liquid into the rotovap that is equal to the amount of liquid dripping from the condenser into the receiving flask. You will know that the input speed and output speed are matched because the chiller will remain at a stable temperature. If the chiller begins to rise, then you are injecting too much liquid. Dial back the valve until the chiller stabilizes.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce everything is stabilized, you may walk away from the rotovap if necessary. Check every so often to make sure temperatures remain stable and evaporation continues efficiently.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cdiv\u003e\u003cstrong\u003e\u003cb\u003e***Note:\u003c\/b\u003e All units are inspected for broken glass or parts before unit is shipped.\u003cb\u003e \u003c\/b\u003eIf unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer \u003cstrong\u003eMUST \u003c\/strong\u003econtact BVV \u003cstrong\u003ewithin 3 days\u003c\/strong\u003e \u003cstrong\u003eof delivery\u003c\/strong\u003e to file a claim and receive a replacement part. If customer \u003cstrong\u003eDOES NOT\u003c\/strong\u003e contact BVV \u003cstrong\u003ewithin 3 days of delivery\u003c\/strong\u003e responsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/div\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cdiv\u003e\u003cstrong\u003e***Note: This item will ship by freight only.***\u003c\/strong\u003e\u003c\/div\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV\u003cstrong\u003e is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Welch BTpro70","offer_id":49567660376375,"sku":"NRE-5L-TK","price":24500.0,"currency_code":"USD","in_stock":true},{"title":"Scroll Pump None","offer_id":49567660409143,"sku":"NRE-5L-TK-NONEUL","price":20500.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/f86347e8e36d53fd8d86a1ea9348beb7.jpg?v=1758127091"},{"product_id":"5l-neocision-etl-lab-certified-rotary-evaporator","title":"BVV - 5L Neocision ETL Lab Certified Rotary Evaporator","description":"\u003ch2\u003e5L Neocision ETL Lab Certified Rotary Evaporator\u003c\/h2\u003e \u003cbr\u003e \u003cp\u003e\u003cspan\u003eThe 5L Neocision ETL Lab Certified Rotary Evaporator is a full-scale system meant to fulfill the needs of large volume production and meet the requirements of a certified laboratory with its ETL certification standards. Featuring an electric lift bath and all PTFE valves for extreme chemical resistance, the 5L Neocision gives users the ability to recover large amounts of solvent in a smaller footprint with highly improved functionality. All Neocision rotovaps feature high-efficiency valves and drain ports making it easy to directly inject solution continuously without the need to stop the system or release vacuum to drain. The temperature and rotation speed are easily controlled from a single digital interface. Our rotovaps are a fraction of the price of more costly systems with the same functionality and evaporation efficiency. \u003c\/span\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cspan\u003e\u003cimg width=\"900\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_rotovapflowchart_jpg?18265071413647998907\" alt=\"Rotovap Flow Chart\" title=\"Rotovap Flow Chart\"\u003e\u003c\/span\u003e\u003c\/p\u003e \u003ch3\u003e\u003cbr\u003e\u003c\/h3\u003e \u003cp\u003e\u003cstrong\u003eFeatures:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eETL Certified for Lab use.\u003c\/li\u003e \u003cli\u003eDigital temperature and speed control with simple user interface\u003c\/li\u003e \u003cli\u003eElectric Bath Lift\u003c\/li\u003e \u003cli\u003eTeflon Coated Bath for corrosion resistance\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eHigh-efficiency drain port and injection valves\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eSmaller footprint for improved workspace allocation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eMobility with locking casters\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eShorter vapor path for faster evaporation and condensation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDirect injection capability for continuous feeding of solution\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eContinuous draining capability without the need to release vacuum or stop the system\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1-year warranty on all mechanical parts. \u003cem\u003eDoes not include glassware. \u003c\/em\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cb\u003eSpecifications:\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e \u003ctable height=\"1537\" border=\"1\"\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eModel\u003c\/b\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003e5L Solvent Pro Series Rotary Evaporator \u003c\/b\u003e\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eOptimum Ambient Temperature\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e5~25C \/ 41~105.8F\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eGlass Material\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eGG-17 High Borosilicate\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003ePower (V\/Hz)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e110V 50\/60Hz Single Phase\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eSpeed Regulation\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eDigital Step-less Regulation\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eRotation Speed\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e20-130 RPM\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eSet Temperature\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eRT+5 - 99C\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eTemperature Control\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eDigital Temperature Control\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eMaximum Vacuum Pressure\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e-29.8 inHg\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eEvaporating Flask Capacity\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e5L (5000ml)\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eReceiving Flask Capacity\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e5L (5000ml)\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eCondenser Style\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eMain + Auxiliary Vertical Double Helix\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eHeater Max Current Draw (Amps)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e25\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWater Bath Material\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e304 Stainless Steel\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWater Bath Size\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e17.7 x 9.8 in.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eLifting Function\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eElectric\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eLifting Stroke\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e190mm \/ 7.5 in.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eTotal Power Consumption (kW)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e1800w\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eDimensions\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e45 x 32 x 15in\u003cbr\u003e\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWeight\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e155 lbs\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eVacuum Connection\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e14mm \/ .55 in. Barb\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eCondenser Connection\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e18mm \/ .70 in. Barb\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWarranty\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e1 Year\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eExcluding: \u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003eMoving Parts \u003cbr\u003e \u003c\/li\u003e \u003cli\u003eGlassware\u003c\/li\u003e \u003c\/ul\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eCertifications\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eETL\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cbr\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eRotovap Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for rotovaps. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs. \u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eClean and assemble unit. Make sure all pieces are cleaned and sterilized using an alcohol solution.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect chiller to condenser and set to 0C (32F). Always fill a rotovap condenser from the top down (chiller output to top of condenser, chiller input to bottom of condenser).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect vacuum pump to cold trap and connect cold trap to vacuum port on rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTurn on heat bath and set to 40C (113F).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce heat bath, chiller and cold trap have reached desired temperatures, turn on rotovap motor and set speed to approximately 100 RPM (does not have to be precise). Keep in mind, higher RPM's will increase evaporation power but also increase heat load.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eStart vacuum pump and allow vacuum to pull down for a few minutes before injection.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce vacuum has been pulled to a sufficient level (does not have to be precise but should be below 100 Torr), using the injection valve, very slowly inject approximately 500 mL of solution into evaporating flask and then close the valve. Allow this small amount to begin evaporating. You may see the chiller begin to rise in temperature, this is called \"priming\" the rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce the temperature stops rising or all liquid is almost completely evaporated, open the injection valve again very slowly so that a small amount of liquid begins to enter the evaporating flask. Do not close injection valve this time but continue to allow solution to enter the evaporating flask.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAt this point you must try to match the input speed to the output speed. What this means is that you should be injecting the same amount of liquid into the rotovap that is equal to the amount of liquid dripping from the condenser into the receiving flask. You will know that the input speed and output speed are matched because the chiller will remain at a stable temperature. If the chiller begins to rise, then you are injecting too much liquid. Dial back the valve until the chiller stabilizes.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce everything is stabilized, you may walk away from the rotovap if necessary. Check every so often to make sure temperatures remain stable and evaporation continues efficiently.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cdiv\u003e\u003cstrong\u003e\u003cb\u003e***Note:\u003c\/b\u003e All units are inspected for broken glass or parts before unit is shipped.\u003cb\u003e \u003c\/b\u003eIf unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer \u003cstrong\u003eMUST \u003c\/strong\u003econtact BVV \u003cstrong\u003ewithin 3 days\u003c\/strong\u003e \u003cstrong\u003eof delivery\u003c\/strong\u003e to file a claim and receive a replacement part. If customer \u003cstrong\u003eDOES NOT\u003c\/strong\u003e contact BVV \u003cstrong\u003ewithin 3 days of delivery\u003c\/strong\u003e responsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/div\u003e \u003cbr\u003e \u003cdiv\u003e\u003cstrong\u003e***Note: This item will ship by freight only.***\u003c\/strong\u003e\u003c\/div\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV\u003cstrong\u003e is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567661949239,"sku":"NRE-5L","price":4000.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/47e5968924eca18b3330e90967c1f560.jpg?v=1758127080"},{"product_id":"10l-neocision-etl-lab-certified-rotary-evaporator","title":"BVV - 10L Neocision ETL Lab Certified Rotary Evaporator","description":"\u003ch2\u003e10L Neocision ETL Lab Certified Rotary Evaporator\u003c\/h2\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003eThe 10L Neocision ETL Lab Certified Rotary Evaporator is a full-scale system meant to fulfill the needs of large volume production and meet the requirements of a certified laboratory with its ETL certification standards. Featuring an electric lift bath and all PTFE valves for extreme chemical resistance, the 10L Neocision gives users the ability to recover large amounts of solvent in a smaller footprint with highly improved functionality. All Neocision rotovaps feature high-efficiency valves and drain ports making it easy to directly inject solution continuously without the need to stop the system or release vacuum to drain. The temperature and rotation speed are easily controlled from a single digital interface. Our rotovaps are a fraction of the price of more costly systems with the same functionality and evaporation efficiency. \u003c\/span\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003e\u003cstrong\u003e\u003ca href=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/10-50L_NEO_and_ECO_Rotary_Evaporator_Diagram.pptx?v=1640096669\" title=\"10-50L BVV Diagram\" target=\"_blank\"\u003e10-50L NEO and ECO Rotary Evaporator Diagram\u003c\/a\u003e\u003c\/strong\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003e\u003cimg width=\"900\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_rotovapflowchart_jpg?18265071413647998907\" alt=\"Rotovap Flow Chart\" title=\"Rotovap Flow Chart\"\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cul\u003e\u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eFeatures:\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eETL Certified for Lab use.\u003c\/li\u003e \u003cli\u003eDigital temperature and speed control with simple user interface\u003c\/li\u003e \u003cli\u003eElectric Bath Lift\u003c\/li\u003e \u003cli\u003eTeflon Coated Bath for corrosion resistance\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eHigh-efficiency drain port and injection valves\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eSmaller footprint for improved workspace allocation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eMobility with locking casters\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eShorter vapor path for faster evaporation and condensation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDirect injection capability for continuous feeding of solution\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eContinuous draining capability without the need to release vacuum or stop the system\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1-year warranty on all mechanical parts. \u003cem\u003eDoes not include glassware. \u003c\/em\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSpecifications:\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003ctable height=\"1525\" border=\"1\"\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eModel\u003c\/b\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003e10L Solvent Pro Series Rotary Evaporator \u003c\/b\u003e\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eOptimum Ambient Temperature\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e5~25C \/ 41~105.8F\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eGlass Material\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eGG-17 High Borosilicate\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003ePower (V\/Hz)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e220-240V 60Hz Single Phase\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eSpeed Regulation\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eDigital Step-less Regulation\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eRotation Speed\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e20-130 RPM\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eSet Temperature\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eRT+5-99C\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eTemperature Control\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eDigital Temperature Control\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eMaximum Vacuum Pressure\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e-29.8 inHg\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eEvaporating Flask Capacity\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e10L (10000ml)\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eReceiving Flask Capacity\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e10L (10000ml)\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eCondenser Style\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eMain + Auxiliary Vertical Double Helix\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eHeater Max Current Draw (Amps)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e25\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWater Bath Material\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e304 Stainless Steel\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWater Bath Size\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e17.7 x 9.8 in.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eLifting Function\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eElectric\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eLifting Stroke\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e190mm \/ 7.5 in.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eTotal Power Consumption (kW)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e3300w\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eDimensions\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e81 x 44 x 20 in.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWeight\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e155 lbs\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eVacuum Connection\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e14mm \/ .55 in. Barb\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eCondenser Connection\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e18mm \/ .70 in. Barb\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWarranty\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e90 days excluding glass parts\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eCertifications\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eETL\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eRotovap Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for rotovaps. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs. \u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eClean and assemble unit. Make sure all pieces are cleaned and sterilized using an alcohol solution.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect chiller to condenser and set to 0C (32F). Always fill a rotovap condenser from the top down (chiller output to top of condenser, chiller input to bottom of condenser).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect vacuum pump to cold trap and connect cold trap to vacuum port on rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTurn on heat bath and set to 40C (113F).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce heat bath, chiller and cold trap have reached desired temperatures, turn on rotovap motor and set speed to approximately 100 RPM (does not have to be precise). Keep in mind, higher RPM's will increase evaporation power but also increase heat load.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eStart vacuum pump and allow vacuum to pull down for a few minutes before injection.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce vacuum has been pulled to a sufficient level (does not have to be precise but should be below 100 Torr), using the injection valve, very slowly inject approximately 500 mL of solution into evaporating flask and then close the valve. Allow this small amount to begin evaporating. You may see the chiller begin to rise in temperature, this is called \"priming\" the rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce the temperature stops rising or all liquid is almost completely evaporated, open the injection valve again very slowly so that a small amount of liquid begins to enter the evaporating flask. Do not close injection valve this time but continue to allow solution to enter the evaporating flask.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAt this point you must try to match the input speed to the output speed. What this means is that you should be injecting the same amount of liquid into the rotovap that is equal to the amount of liquid dripping from the condenser into the receiving flask. You will know that the input speed and output speed are matched because the chiller will remain at a stable temperature. If the chiller begins to rise, then you are injecting too much liquid. Dial back the valve until the chiller stabilizes.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce everything is stabilized, you may walk away from the rotovap if necessary. Check every so often to make sure temperatures remain stable and evaporation continues efficiently.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cdiv\u003e\u003cstrong\u003e\u003cb\u003e***Note:\u003c\/b\u003e All units are inspected for broken glass or parts before unit is shipped.\u003cb\u003e \u003c\/b\u003eIf unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer \u003cstrong\u003eMUST \u003c\/strong\u003econtact BVV \u003cstrong\u003ewithin 3 days\u003c\/strong\u003e \u003cstrong\u003eof delivery\u003c\/strong\u003e to file a claim and receive a replacement part. If customer \u003cstrong\u003eDOES NOT\u003c\/strong\u003e contact BVV \u003cstrong\u003ewithin 3 days of delivery\u003c\/strong\u003e responsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/div\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cdiv\u003e\u003cstrong\u003e***Note: This item will ship by freight only.***\u003c\/strong\u003e\u003c\/div\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV\u003cstrong\u003e is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e\u003cstrong\u003e\u003ciframe src=\"https:\/\/www.youtube.com\/embed\/0H2-K6F7jqc\" height=\"315\" width=\"560\" allowfullscreen=\"\" allow=\"accelerometer; autoplay; encrypted-media; gyroscope; picture-in-picture\" frameborder=\"0\"\u003e\u003c\/iframe\u003e\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567663587639,"sku":"NRE-10L","price":4000.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/4d1d41760f5e6dc77fed6f5f0c5f1b86.jpg?v=1758126802"},{"product_id":"50l-neo-rotary-evaporator-turnkey-system","title":"BVV - 50L Neocision ETL Lab Certified Rotary Evaporator Turnkey System","description":"\u003ch2\u003e50L Neocision ETL Lab Certified Rotary Evaporator Turnkey System\u003c\/h2\u003e \u003cp\u003e\u003cspan\u003e50L NEO Rotary Evaporator Turnkey System \u003cspan\u003esetup includes all the necessary components to successfully perform solvent recovery via rotary evaporation. A cold trap should always be used inline between your vacuum system and application to protect the pump from volatile vapors.\u003c\/span\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003e\u003cstrong\u003e\u003ca href=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/10-50L_NEO_and_ECO_Rotary_Evaporator_Diagram.pptx?v=1640096669\" title=\"10-50L BVV Diagram\" target=\"_blank\"\u003e10-50L NEO and ECO Rotary Evaporator Diagram\u003c\/a\u003e\u003c\/strong\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003cspan\u003e\u003cimg height=\"454\" width=\"808\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_rotovapflowchart_jpg?130795633027647600\" alt=\"Rotovap Flow Chart\" title=\"Rotovap Flow Chart\"\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e50L NEO Rotary Evaporator Turnkey System setup includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003e50L Neocision ETL Lab Certified Rotary Evaporator\u003cbr\u003e \u003c\/li\u003e \u003cli\u003e\u003ca title=\"Polyscience 1.5HP Durachill\" href=\"https:\/\/shopbvv.com\/products\/polyscience-durachill-10c-1-5hp-chiller-w-turbine-pump\" target=\"_blank\"\u003ePolyscience DuraChill 1.5HP Chiller w\/ Turbine Pump\u003c\/a\u003e\u003c\/li\u003e \u003cli\u003e3\/8\" Gum Rubber - 100ft\u003cbr\u003e \u003c\/li\u003e \u003cli\u003e3\/8\" Silicone Tubing - 25ft\u003c\/li\u003e \u003cli\u003e \u003ca title=\"Welch BTPRO100\" href=\"https:\/\/shopbvv.com\/products\/welch-btpro100\" target=\"_blank\"\u003eWelch BTpro100 Diaphragm Pump\u003c\/a\u003e\u003cbr\u003e \u003c\/li\u003e \u003cli\u003eAdjustable Stainless Steel Hose Clamps\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for rotovaps. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cul\u003e \u003cli\u003eClean and assemble unit. Make sure all pieces are cleaned and sterilized using an alcohol solution.\u003c\/li\u003e \u003cli\u003e Connect chiller to condenser and set to 0C (32F). Always fill a rotovap condenser from the top down (chiller output to top of condenser, chiller input to bottom of condenser).\u003c\/li\u003e \u003cli\u003e Connect vacuum pump to cold trap and connect cold trap to vacuum port on rotovap.\u003c\/li\u003e \u003cli\u003e Turn on heat bath and set to 40C (113F).\u003c\/li\u003e \u003cli\u003e Once heat bath, chiller and cold trap have reached desired temperatures, turn on rotovap motor and set speed to approximately 100 RPM (does not have to be precise). Keep in mind, higher RPM's will increase evaporation power but also increase heat load.\u003c\/li\u003e \u003cli\u003e Start vacuum pump and allow vacuum to pull down for a few minutes before injection.\u003c\/li\u003e \u003cli\u003e Once vacuum has been pulled to a sufficient level (does not have to be precise but should be below 100 Torr), using the injection valve, very slowly inject approximately 500 mL of solution into evaporating flask and then close the valve. Allow this small amount to begin evaporating. You may see the chiller begin to rise in temperature, this is called \"priming\" the rotovap.\u003c\/li\u003e \u003cli\u003e Once the temperature stops rising or all liquid is almost completely evaporated, open the injection valve again very slowly so that a small amount of liquid begins to enter the evaporating flask. Do not close injection valve this time but continue to allow solution to enter the evaporating flask.\u003c\/li\u003e \u003cli\u003e At this point you must try to match the input speed to the output speed. What this means is that you should be injecting the same amount of liquid into the rotovap that is equal to the amount of liquid dripping from the condenser into the receiving flask. You will know that the input speed and output speed are matched because the chiller will remain at a stable temperature. If the chiller begins to rise, then you are injecting too much liquid. Dial back the valve until the chiller stabilizes.\u003c\/li\u003e \u003cli\u003e Once everything is stabilized, you may walk away from the rotovap if necessary. Check every so often to make sure temperatures remain stable and evaporation continues efficiently.\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003ciframe src=\"https:\/\/www.youtube.com\/embed\/0H2-K6F7jqc\" height=\"315\" width=\"560\" allowfullscreen=\"\" allow=\"accelerometer; autoplay; encrypted-media; gyroscope; picture-in-picture\" frameborder=\"0\"\u003e\u003c\/iframe\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Welch BTpro100 Diaphragm Pump","offer_id":49567666209079,"sku":"NRE-50L-TK","price":22500.0,"currency_code":"USD","in_stock":true},{"title":"Scroll Pump Non","offer_id":49567666241847,"sku":"NRE-50L-TK-NONEUL","price":19750.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/33b52f6dacdc1e75081f68bc68458429.jpg?v=1758127031"},{"product_id":"20l-neo-rotary-evaporator-turnkey-system","title":"BVV - 20L Neocision ETL Lab Certified Rotary Evaporator Turnkey System","description":"\u003ch2\u003e20L Neocision ETL Lab Certified Rotary Evaporator Turnkey System\u003c\/h2\u003e \u003cp\u003e\u003cspan\u003e20L NEO Rotary Evaporator Turnkey System \u003c\/span\u003esetup includes all the necessary components to successfully perform solvent recovery via rotary evaporation. A cold trap should always be used inline between your vacuum system and application to protect the pump from volatile vapors.\u003c\/p\u003e \u003cul\u003e \u003cli\u003e\u003cstrong\u003e\u003ca title=\"10-50L BVV Diagram\" href=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/10-50L_NEO_and_ECO_Rotary_Evaporator_Diagram.pptx?v=1640096669\" target=\"_blank\"\u003e10-50L NEO and ECO Rotary Evaporator Diagram\u003c\/a\u003e\u003c\/strong\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003cimg height=\"306\" width=\"545\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_rotovapflowchart_jpg?130795633027647600\" alt=\"Rotovap Flow Chart\" title=\"Rotovap Flow Chart\"\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e20L NEO Rotary Evaporator Turnkey System setup includes:\u003c\/strong\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003e20L Neocision ETL Lab Certified Rotary Evaporator\u003cbr\u003e \u003c\/li\u003e \u003cli\u003e\u003ca title=\"Polyscience 6160T\" href=\"https:\/\/shopbvv.com\/products\/polyscience-6160-10c-4-2l-1hp-chiller-w-turbine-pump-100-psi\" target=\"_blank\"\u003ePolyscience 6160T 1HP Chiller\u003c\/a\u003e\u003c\/li\u003e \u003cli\u003e3\/8\" Gum Rubber - 100ft\u003cbr\u003e \u003c\/li\u003e \u003cli\u003e3\/8\" Silicone Tubing - 25ft\u003c\/li\u003e \u003cli\u003e \u003ca title=\"Welch BTPRO 100\" href=\"https:\/\/shopbvv.com\/products\/welch-btpro100\" target=\"_blank\"\u003eWelch BTpro100 Diaphragm Pump\u003c\/a\u003e\u003cbr\u003e \u003c\/li\u003e \u003cli\u003eAdjustable Stainless Steel Hose Clamps\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003cb\u003eRotovap Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for rotovaps. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eClean and assemble unit. Make sure all pieces are cleaned and sterilized using an alcohol solution.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect chiller to condenser and set to 0C (32F). Always fill a rotovap condenser from the top down (chiller output to top of condenser, chiller input to bottom of condenser).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect vacuum pump to cold trap and connect cold trap to vacuum port on rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTurn on heat bath and set to 40C (113F).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce heat bath, chiller and cold trap have reached desired temperatures, turn on rotovap motor and set speed to approximately 100 RPM (does not have to be precise). Keep in mind, higher RPM's will increase evaporation power but also increase heat load.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eStart vacuum pump and allow vacuum to pull down for a few minutes before injection.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce vacuum has been pulled to a sufficient level (does not have to be precise but should be below 100 Torr), using the injection valve, very slowly inject approximately 500 mL of solution into evaporating flask and then close the valve. Allow this small amount to begin evaporating. You may see the chiller begin to rise in temperature, this is called \"priming\" the rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce the temperature stops rising or all liquid is almost completely evaporated, open the injection valve again very slowly so that a small amount of liquid begins to enter the evaporating flask. Do not close injection valve this time but continue to allow solution to enter the evaporating flask.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAt this point you must try to match the input speed to the output speed. What this means is that you should be injecting the same amount of liquid into the rotovap that is equal to the amount of liquid dripping from the condenser into the receiving flask. You will know that the input speed and output speed are matched because the chiller will remain at a stable temperature. If the chiller begins to rise, then you are injecting too much liquid. Dial back the valve until the chiller stabilizes.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce everything is stabilized, you may walk away from the rotovap if necessary. Check every so often to make sure temperatures remain stable and evaporation continues efficiently.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cdiv\u003e\u003cstrong\u003e\u003cb\u003e***Note:\u003c\/b\u003e\u003cspan\u003e \u003c\/span\u003eAll units are inspected for broken glass or parts before unit is shipped.\u003cb\u003e\u003cspan\u003e \u003c\/span\u003e\u003c\/b\u003eIf unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer\u003cspan\u003e \u003c\/span\u003eMUST\u003cspan\u003e \u003c\/span\u003econtact BVV within 3 days\u003cspan\u003e \u003c\/span\u003eof delivery\u003cspan\u003e \u003c\/span\u003eto file a claim and receive a replacement part. If customer\u003cspan\u003e \u003c\/span\u003eDOES NOT\u003cspan\u003e \u003c\/span\u003econtact BVV within 3 days of delivery\u003cspan\u003e \u003c\/span\u003eresponsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/div\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cdiv\u003e\u003cstrong\u003e***Note: This item will ship by freight only.***\u003c\/strong\u003e\u003c\/div\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e\u003ciframe src=\"https:\/\/www.youtube.com\/embed\/0H2-K6F7jqc\" height=\"315\" width=\"560\" allowfullscreen=\"\" allow=\"accelerometer; autoplay; encrypted-media; gyroscope; picture-in-picture\" frameborder=\"0\"\u003e\u003c\/iframe\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Welch BTpro100 Diaphragm Pump","offer_id":49567667945783,"sku":"NRE-20L-TK","price":31149.0,"currency_code":"USD","in_stock":true},{"title":"Scroll Pump Non","offer_id":49567667978551,"sku":"NRE-20L-TK-NONEUL","price":26910.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/c31493277bee28c000c988c4e9466128.jpg?v=1758126921"},{"product_id":"10l-neo-rotary-evaporator-turnkey-system","title":"BVV - 10L Neocision ETL Lab Certified Rotary Evaporator Turnkey System","description":"\u003ch2\u003e\u003cspan\u003e10L NEO Rotary Evaporator Turnkey System\u003c\/span\u003e\u003c\/h2\u003e \u003cp\u003e\u003cspan\u003e10L NEO Rotary Evaporator Turnkey System \u003cspan\u003esetup includes all the necessary components to successfully perform solvent recovery via rotary evaporation. A cold trap should always be used inline between your vacuum system and application to protect the pump from volatile vapors.\u003c\/span\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003e\u003cstrong\u003e\u003ca title=\"10-50L BVV Diagram\" href=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/10-50L_NEO_and_ECO_Rotary_Evaporator_Diagram.pptx?v=1640096669\" target=\"_blank\"\u003e10-50L NEO and ECO Rotary Evaporator Diagram\u003c\/a\u003e\u003c\/strong\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003e\u003cspan\u003e\u003cimg title=\"Rotovap Flow Chart\" alt=\"Rotovap Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_rotovapflowchart_jpg?130795633027647600\" width=\"808\" height=\"454\"\u003e\u003c\/span\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e10L NEO Rotary Evaporator Turnkey System setup includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003e10L Neocision ETL Lab Certified Rotary Evaporator\u003cbr\u003e \u003c\/li\u003e \u003cli\u003e\u003ca href=\"https:\/\/shopbvv.com\/products\/polyscience-6160-10c-4-2l-1hp-chiller-w-turbine-pump-100-psi\" title=\"Polyscience 6160T\" target=\"_blank\"\u003ePolyscience 6160T 1HP Chiller\u003c\/a\u003e\u003c\/li\u003e \u003cli\u003e3\/8\" Gum Rubber - 100ft\u003cbr\u003e \u003c\/li\u003e \u003cli\u003e3\/8\" Silicone Tubing - 25ft\u003c\/li\u003e \u003cli\u003e\u003ca href=\"https:\/\/shopbvv.com\/products\/welch-btpro100\" title=\"Welch BTPRO 100\" target=\"_blank\"\u003eWelch BTpro100 Diaphragm Pump\u003c\/a\u003e\u003c\/li\u003e \u003cli\u003eAdjustable Stainless Steel Hose Clamps\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for rotovaps. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003eClean and assemble unit. Make sure all pieces are cleaned and sterilized using an alcohol solution.\u003c\/li\u003e \u003cli\u003e Connect chiller to condenser and set to 0C (32F). Always fill a rotovap condenser from the top down (chiller output to top of condenser, chiller input to bottom of condenser).\u003c\/li\u003e \u003cli\u003e Connect vacuum pump to cold trap and connect cold trap to vacuum port on rotovap.\u003c\/li\u003e \u003cli\u003e Turn on heat bath and set to 40C (113F).\u003c\/li\u003e \u003cli\u003e Once heat bath, chiller and cold trap have reached desired temperatures, turn on rotovap motor and set speed to approximately 100 RPM (does not have to be precise). Keep in mind, higher RPM's will increase evaporation power but also increase heat load.\u003c\/li\u003e \u003cli\u003e Start vacuum pump and allow vacuum to pull down for a few minutes before injection.\u003c\/li\u003e \u003cli\u003e Once vacuum has been pulled to a sufficient level (does not have to be precise but should be below 100 Torr), using the injection valve, very slowly inject approximately 500 mL of solution into evaporating flask and then close the valve. Allow this small amount to begin evaporating. You may see the chiller begin to rise in temperature, this is called \"priming\" the rotovap.\u003c\/li\u003e \u003cli\u003e Once the temperature stops rising or all liquid is almost completely evaporated, open the injection valve again very slowly so that a small amount of liquid begins to enter the evaporating flask. Do not close injection valve this time but continue to allow solution to enter the evaporating flask.\u003c\/li\u003e \u003cli\u003e At this point you must try to match the input speed to the output speed. What this means is that you should be injecting the same amount of liquid into the rotovap that is equal to the amount of liquid dripping from the condenser into the receiving flask. You will know that the input speed and output speed are matched because the chiller will remain at a stable temperature. If the chiller begins to rise, then you are injecting too much liquid. Dial back the valve until the chiller stabilizes.\u003c\/li\u003e \u003cli\u003e Once everything is stabilized, you may walk away from the rotovap if necessary. Check every so often to make sure temperatures remain stable and evaporation continues efficiently.\u003c\/li\u003e \u003c\/ul\u003e \u003cdiv\u003e\u003cstrong\u003e\u003cb\u003e**Note:\u003c\/b\u003e\u003cspan\u003e \u003c\/span\u003eAll units are inspected for broken glass or parts before unit is shipped.\u003cb\u003e\u003cspan\u003e \u003c\/span\u003e\u003c\/b\u003eIf unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer\u003cspan\u003e \u003c\/span\u003eMUST\u003cspan\u003e \u003c\/span\u003econtact BVV within 3 days\u003cspan\u003e \u003c\/span\u003eof delivery\u003cspan\u003e \u003c\/span\u003eto file a claim and receive a replacement part. If customer\u003cspan\u003e \u003c\/span\u003eDOES NOT\u003cspan\u003e \u003c\/span\u003econtact BVV within 3 days of delivery\u003cspan\u003e \u003c\/span\u003eresponsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/div\u003e \u003cp\u003e\u003cstrong\u003e \u003c\/strong\u003e\u003c\/p\u003e \u003cdiv\u003e\u003cstrong\u003e***Note: This item will ship by freight only.***\u003c\/strong\u003e\u003c\/div\u003e \u003cp\u003e\u003cstrong\u003e \u003c\/strong\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cstrong\u003e \u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e\u003ciframe width=\"560\" height=\"315\" src=\"https:\/\/www.youtube.com\/embed\/0H2-K6F7jqc\" allowfullscreen=\"\" allow=\"accelerometer; autoplay; encrypted-media; gyroscope; picture-in-picture\" frameborder=\"0\"\u003e\u003c\/iframe\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Welch BTpro100 Diaphragm Pump","offer_id":49567670305079,"sku":"NRE-10L-TK","price":30010.0,"currency_code":"USD","in_stock":true},{"title":"Scroll Pump Non","offer_id":49567670337847,"sku":"NRE-10L-TK-NONEUL","price":24900.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/37c52f585a0f70173d62d9e2810e4d70.jpg?v=1758126837"},{"product_id":"50l-neocision-etl-lab-certified-rotary-evaporator","title":"BVV - 50L Neocision ETL Lab Certified Rotary Evaporator","description":"\u003ch2\u003e50L Neocision ETL Lab Certified Rotary Evaporator\u003c\/h2\u003e \u003cbr\u003e \u003cp\u003e\u003cspan\u003eThe 50L Neocision ETL Lab Certified Rotary Evaporator is a full-scale system meant to fulfill the needs of large volume production and meet the requirements of a certified laboratory with its ETL certification standards. Featuring an electric lift bath and all PTFE valves for extreme chemical resistance, the 50L Neocision gives users the ability to recover large amounts of solvent in a smaller footprint with highly improved functionality. All Neocision rotovaps feature high-efficiency valves and drain ports making it easy to directly inject solution continuously without the need to stop the system or release vacuum to drain. The temperature and rotation speed are easily controlled from a single digital interface. Our rotovaps are a fraction of the price of more costly systems with the same functionality and evaporation efficiency. \u003c\/span\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003e\u003cstrong\u003e\u003ca title=\"10-50L BVV Diagram\" href=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/10-50L_NEO_and_ECO_Rotary_Evaporator_Diagram.pptx?v=1640096669\" target=\"_blank\"\u003e10-50L NEO and ECO Rotary Evaporator Diagram\u003c\/a\u003e\u003c\/strong\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cp\u003e \u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cspan\u003e\u003cimg title=\"Rotovap Flow Chart\" alt=\"Rotovap Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_rotovapflowchart_jpg?18265071413647998907\" width=\"900\"\u003e\u003c\/span\u003e\u003c\/p\u003e \u003ch3\u003e\u003cbr\u003e\u003c\/h3\u003e \u003cp\u003e\u003cstrong\u003eFeatures:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eETL Certified for Lab use.\u003c\/li\u003e \u003cli\u003eDigital temperature and speed control with simple user interface\u003c\/li\u003e \u003cli\u003eElectric Bath Lift\u003c\/li\u003e \u003cli\u003eTeflon Coated Bath for corrosion resistance\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eHigh-efficiency drain port and injection valves\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eSmaller footprint for improved workspace allocation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eMobility with locking casters\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eShorter vapor path for faster evaporation and condensation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDirect injection capability for continuous feeding of solution\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eContinuous draining capability without the need to release vacuum or stop the system\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1-year warranty on all mechanical parts. \u003cem\u003eDoes not include glassware\/moving parts\u003c\/em\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cb\u003eSpecifications:\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e \u003ctable border=\"1\"\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eModel\u003c\/b\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003e50L NEOCISION Rotary Evaporator \u003c\/b\u003e\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eOptimum Ambient Temperature\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e5~25C \/ 41~105.8F\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eGlass Material\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eGG-17 High Borosilicate\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003ePower (V\/Hz)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e220-240V 60Hz Single Phase\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eSpeed Regulation\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eDigital Step-less Regulation\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eRotation Speed\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e0-120 RPM\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eSet Temperature\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e0-99C \/ 0-210F\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eTemperature Control\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eDigital Temperature Control\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eMaximum Vacuum Pressure\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e-29.8 inHg\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eEvaporating Flask Capacity\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e50L (20000ml)\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eReceiving Flask Capacity\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e20L (10000ml)\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eCondenser Style\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eMain + Auxiliary Vertical Double Helix\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eEvaporation Capacity\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eAlcohol \u0026gt;\/= 12 L\/H\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eHeater Max Current Draw (Amps)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e25\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWater Bath Material\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e304 Stainless Steel\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWater Bath Size\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e17.7 x 9.8 in.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eLifting Function\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eElectric\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eLifting Stroke\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e190mm \/ 7.5 in.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eTotal Power Consumption (kW)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e4.1 kW\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eDimensions\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e49 x 24 x 83 in.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWeight\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e155 lbs\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eVacuum Connection\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e10mm \/ 3\/8 in. Barb\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eCondenser Connection\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e10mm \/ 3\/8 in. Barb\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eWarranty\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e1 Year\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eExcluding:\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003eMoving Parts\u003c\/li\u003e \u003cli\u003e\u003cspan\u003eGlassware\u003c\/span\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eCertifications\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cbr\u003e \u003cp\u003eETL\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cbr\u003e \u003cp\u003e \u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eRotovap Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for rotovaps. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs. \u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eClean and assemble unit. Make sure all pieces are cleaned and sterilized using an alcohol solution.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect chiller to condenser and set to 0C (32F). Always fill a rotovap condenser from the top down (chiller output to top of condenser, chiller input to bottom of condenser).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect vacuum pump to cold trap and connect cold trap to vacuum port on rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTurn on heat bath and set to 40C (113F).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce heat bath, chiller and cold trap have reached desired temperatures, turn on rotovap motor and set speed to approximately 100 RPM (does not have to be precise). Keep in mind, higher RPM's will increase evaporation power but also increase heat load.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eStart vacuum pump and allow vacuum to pull down for a few minutes before injection.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce vacuum has been pulled to a sufficient level (does not have to be precise but should be below 100 Torr), using the injection valve, very slowly inject approximately 500 mL of solution into evaporating flask and then close the valve. Allow this small amount to begin evaporating. You may see the chiller begin to rise in temperature, this is called \"priming\" the rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce the temperature stops rising or all liquid is almost completely evaporated, open the injection valve again very slowly so that a small amount of liquid begins to enter the evaporating flask. Do not close injection valve this time but continue to allow solution to enter the evaporating flask.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAt this point you must try to match the input speed to the output speed. What this means is that you should be injecting the same amount of liquid into the rotovap that is equal to the amount of liquid dripping from the condenser into the receiving flask. You will know that the input speed and output speed are matched because the chiller will remain at a stable temperature. If the chiller begins to rise, then you are injecting too much liquid. Dial back the valve until the chiller stabilizes.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce everything is stabilized, you may walk away from the rotovap if necessary. Check every so often to make sure temperatures remain stable and evaporation continues efficiently.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cdiv\u003e\u003cstrong\u003e\u003cb\u003e***Note:\u003c\/b\u003e All units are inspected for broken glass or parts before unit is shipped.\u003cb\u003e \u003c\/b\u003eIf unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer \u003cstrong\u003eMUST \u003c\/strong\u003econtact BVV \u003cstrong\u003ewithin 3 days\u003c\/strong\u003e \u003cstrong\u003eof delivery\u003c\/strong\u003e to file a claim and receive a replacement part. If customer \u003cstrong\u003eDOES NOT\u003c\/strong\u003e contact BVV \u003cstrong\u003ewithin 3 days of delivery\u003c\/strong\u003e responsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/div\u003e \u003cbr\u003e \u003cdiv\u003e\u003cstrong\u003e***Note: This item will ship by freight only.***\u003c\/strong\u003e\u003c\/div\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV\u003cstrong\u003e is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***.\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e\u003cstrong\u003e\u003ciframe width=\"560\" height=\"315\" src=\"https:\/\/www.youtube.com\/embed\/0H2-K6F7jqc\" frameborder=\"0\" allow=\"accelerometer; autoplay; encrypted-media; gyroscope; picture-in-picture\" allowfullscreen=\"\"\u003e\u003c\/iframe\u003e\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567680790839,"sku":"NRE-50L","price":7250.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/fa221c7bace5d97d05d128cd35bdb73f.jpg?v=1758126991"},{"product_id":"20l-neocision-etl-lab-certified-rotary-evaporator","title":"BVV - 20L Neocision ETL Lab Certified Rotary Evaporator","description":"\u003ch2\u003e20L Neocision ETL Lab Certified Rotary Evaporator\u003c\/h2\u003e \u003cbr\u003e \u003cp\u003e\u003cspan\u003eThe 20L Neocision ETL Lab Certified Rotary Evaporator is a full-scale system meant to fulfill the needs of large volume production and meet the requirements of a certified laboratory with its ETL certification standards. Featuring an electric lift bath and all PTFE valves for extreme chemical resistance, the 20L Neocision gives users the ability to recover large amounts of solvent in a smaller footprint with highly improved functionality. All Neocision rotovaps feature high-efficiency valves and drain ports making it easy to directly inject solution continuously without the need to stop the system or release vacuum to drain. The temperature and rotation speed are easily controlled from a single digital interface. Our rotovaps are a fraction of the price of more costly systems with the same functionality and evaporation efficiency. \u003c\/span\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003e\u003cstrong\u003e\u003ca title=\"10-50L BVV Diagram\" href=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/10-50L_NEO_and_ECO_Rotary_Evaporator_Diagram.pptx?v=1640096669\" target=\"_blank\"\u003e10-50L NEO and ECO Rotary Evaporator Diagram\u003c\/a\u003e\u003c\/strong\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cp\u003e \u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cspan\u003e\u003cimg title=\"Rotovap Flow Chart\" alt=\"Rotovap Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_rotovapflowchart_jpg?18265071413647998907\" width=\"900\"\u003e\u003c\/span\u003e\u003c\/p\u003e \u003ch3\u003e\u003cbr\u003e\u003c\/h3\u003e \u003cp\u003e\u003cstrong\u003eFeatures:\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003eETL Certified for Lab use.\u003c\/li\u003e \u003cli\u003eDigital temperature and speed control with simple user interface\u003c\/li\u003e \u003cli\u003eElectric Bath Lift\u003c\/li\u003e \u003cli\u003eTeflon Coated Bath for corrosion resistance\u003c\/li\u003e \u003cli\u003eHigh-efficiency drain port and injection valves\u003c\/li\u003e \u003cli\u003eSmaller footprint for improved workspace allocation\u003c\/li\u003e \u003cli\u003eMobility with locking casters\u003c\/li\u003e \u003cli\u003eShorter vapor path for faster evaporation and condensation\u003c\/li\u003e \u003cli\u003eDirect injection capability for continuous feeding of solution\u003c\/li\u003e \u003cli\u003eContinuous draining capability without the need to release vacuum or stop the system\u003c\/li\u003e \u003cli\u003e1-year warranty on all mechanical parts. \u003cem\u003eDoes not include glassware.\u003c\/em\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e \u003c\/p\u003e \u003cul\u003e\u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003ctable\u003e \u003ccolgroup\u003e \u003ccol\u003e \u003ccol\u003e \u003c\/colgroup\u003e \u003cthead\u003e \u003ctr\u003e \u003cth\u003eModel\u003c\/th\u003e \u003cth\u003e20L NEOCISION Rotary Evaporator\u003c\/th\u003e \u003c\/tr\u003e \u003c\/thead\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd\u003eOptimum Ambient Temperature\u003c\/td\u003e \u003ctd\u003e5~25C \/ 41~105.8F\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eGlass Material\u003c\/td\u003e \u003ctd\u003eGG-17 High Borosilicate\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003ePower (V\/Hz)\u003c\/td\u003e \u003ctd\u003e220-240V 60Hz Single Phase\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eSpeed Regulation\u003c\/td\u003e \u003ctd\u003eDigital Step-less Regulation\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eRotation Speed\u003c\/td\u003e \u003ctd\u003e0-120 RPM\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eSet Temperature\u003c\/td\u003e \u003ctd\u003e0-99C \/ 0-210F\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eTemperature Control\u003c\/td\u003e \u003ctd\u003eDigital Temperature Control\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eMaximum Vacuum Pressure\u003c\/td\u003e \u003ctd\u003e-29.8 inHg\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eEvaporating Flask Capacity\u003c\/td\u003e \u003ctd\u003e20L (20000ml)\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eReceiving Flask Capacity\u003c\/td\u003e \u003ctd\u003e10L (10000ml)\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eCondenser Style\u003c\/td\u003e \u003ctd\u003eMain + Auxiliary Vertical Double Helix\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eEvaporation Capacity\u003c\/td\u003e \u003ctd\u003eAlcohol \u0026gt;\/= 12 L\/H\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eHeater Max Current Draw (Amps)\u003c\/td\u003e \u003ctd\u003e25\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eWater Bath Material\u003c\/td\u003e \u003ctd\u003e304 Stainless Steel\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eWater Bath Size\u003c\/td\u003e \u003ctd\u003e17.7 x 9.8 in.\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eLifting Function\u003c\/td\u003e \u003ctd\u003eElectric\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eLifting Stroke\u003c\/td\u003e \u003ctd\u003e190mm \/ 7.5 in.\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eTotal Power Consumption (kW)\u003c\/td\u003e \u003ctd\u003e4.1\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eDimensions\u003c\/td\u003e \u003ctd\u003e49 x 24 x 83 in.\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eWeight\u003c\/td\u003e \u003ctd\u003e155 lbs\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eVacuum Connection\u003c\/td\u003e \u003ctd\u003e10mm \/ 3\/8 in. Barb\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eCondenser Connection\u003c\/td\u003e \u003ctd\u003e10mm \/ 3\/8 in. Barb\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eWarranty\u003c\/td\u003e \u003ctd\u003e1 Year excluding glass parts\u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003eCertifications\u003c\/td\u003e \u003ctd\u003eETL\u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cp\u003e\u003cbr\u003e \u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003e\u003cb\u003eRotovap Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for rotovaps. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs.\u003c\/b\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003eClean and assemble unit. Make sure all pieces are cleaned and sterilized using an alcohol solution.\u003c\/li\u003e \u003cli\u003eConnect chiller to condenser and set to 0C (32F). Always fill a rotovap condenser from the top down (chiller output to top of condenser, chiller input to bottom of condenser).\u003c\/li\u003e \u003cli\u003eConnect vacuum pump to cold trap and connect cold trap to vacuum port on rotovap.\u003c\/li\u003e \u003cli\u003eTurn on heat bath and set to 40C (113F).\u003c\/li\u003e \u003cli\u003eOnce heat bath, chiller and cold trap have reached desired temperatures, turn on rotovap motor and set speed to approximately 100 RPM (does not have to be precise). Keep in mind, higher RPM's will increase evaporation power but also increase heat load.\u003c\/li\u003e \u003cli\u003eStart vacuum pump and allow vacuum to pull down for a few minutes before injection.\u003c\/li\u003e \u003cli\u003eOnce vacuum has been pulled to a sufficient level (does not have to be precise but should be below 100 Torr), using the injection valve, very slowly inject approximately 500 mL of solution into evaporating flask and then close the valve. Allow this small amount to begin evaporating. You may see the chiller begin to rise in temperature, this is called \"priming\" the rotovap.\u003c\/li\u003e \u003cli\u003eOnce the temperature stops rising or all liquid is almost completely evaporated, open the injection valve again very slowly so that a small amount of liquid begins to enter the evaporating flask. Do not close injection valve this time but continue to allow solution to enter the evaporating flask.\u003c\/li\u003e \u003cli\u003eAt this point you must try to match the input speed to the output speed. What this means is that you should be injecting the same amount of liquid into the rotovap that is equal to the amount of liquid dripping from the condenser into the receiving flask. You will know that the input speed and output speed are matched because the chiller will remain at a stable temperature. If the chiller begins to rise, then you are injecting too much liquid. Dial back the valve until the chiller stabilizes.\u003c\/li\u003e \u003cli\u003eOnce everything is stabilized, you may walk away from the rotovap if necessary. Check every so often to make sure temperatures remain stable and evaporation continues efficiently.\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e \u003c\/p\u003e \u003cul\u003e\u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cdiv\u003e\u003cstrong\u003e\u003cb\u003e***Note:\u003c\/b\u003e All units are inspected for broken glass or parts before unit is shipped.\u003cb\u003e \u003c\/b\u003eIf unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer \u003cstrong\u003eMUST \u003c\/strong\u003econtact BVV \u003cstrong\u003ewithin 3 days\u003c\/strong\u003e \u003cstrong\u003eof delivery\u003c\/strong\u003e to file a claim and receive a replacement part. If customer \u003cstrong\u003eDOES NOT\u003c\/strong\u003e contact BVV \u003cstrong\u003ewithin 3 days of delivery\u003c\/strong\u003e responsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/div\u003e \u003cbr\u003e \u003cdiv\u003e\u003cstrong\u003e***Note: This item will ship by freight only.***\u003c\/strong\u003e\u003c\/div\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV\u003cstrong\u003e is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e\u003cstrong\u003e\u003ciframe width=\"560\" height=\"315\" src=\"https:\/\/www.youtube.com\/embed\/0H2-K6F7jqc\" frameborder=\"0\" allow=\"accelerometer; autoplay; encrypted-media; gyroscope; picture-in-picture\" allowfullscreen=\"\"\u003e\u003c\/iframe\u003e\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567688982839,"sku":"NRE-20L","price":5500.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/7034cfe87d667a55ce1dea50b7b279d8.jpg?v=1758126881"},{"product_id":"10l-premium-short-path-distillation-turnkey-system","title":"BVV - 10L Premium Short Path Distillation Turnkey System","description":"\u003ch2\u003e10L Premium Short Path Distillation Turnkey System\u003c\/h2\u003e \u003cp\u003e\u003cspan\u003e\u003cem\u003eThis unit carries\u003cspan\u003e \u003c\/span\u003ea 2 day lead time.\u003c\/em\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003e\u003cem\u003e(Note: Stainless Steel Table NOT Included.)\u003c\/em\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003eThe 10L Premium Short Path Distillation Turnkey System features our USA made \u003cspan\u003eP10 Distillation Head.\u003c\/span\u003e Every component in this turnkey is made for precision, throughput, and repeatable results. Also included the Kangaroo digital thermometer which is very rugged and reliable. You will also receive a Ribbed Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. \u003cspan\u003eThis Turnkey Setup gives you everything needed to perform distillation at the highest level.\u003c\/span\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cimg title=\"Distillation Flow Chart\" alt=\"Distillation Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/5\/assets\/description_image_distillationdiagramfinal_jpg?7355035109499693479\" width=\"900\"\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eThe 10L Neo Kit Includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10L Short Path Distillation Kit including glassware, labware, and P10 Distillation Head.\u003c\/li\u003e \u003cli\u003e10L Digital Heating and Stirring Mantle.\u003c\/li\u003e \u003cli\u003ePolyscience 15 Liter Advanced Digital Heated Circulator\u003c\/li\u003e \u003cli\u003eBVV 21.2CFM Pro Series Corrosion Resistant Vacuum Pump\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eValved Vacuum Adapter.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRibbed Dewar Style Glass Cold Trap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eKangaroo Digital Thermometer.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003cli\u003eOnce process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003col\u003e\u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Note: This entire setup will ship via motor freight.***\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV\u003cstrong\u003e is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e\u003cstrong\u003e\u003ciframe width=\"560\" height=\"315\" src=\"https:\/\/www.youtube.com\/embed\/Bi4sVnTv1S0\" frameborder=\"0\" allow=\"accelerometer; autoplay; encrypted-media; gyroscope; picture-in-picture\" allowfullscreen=\"\"\u003e\u003c\/iframe\u003e\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567694422327,"sku":"10LP10TK","price":11500.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/52b92e43f58a4d52a9c209dec1419f73.jpg?v=1758128012"},{"product_id":"20l-neocision-dual-short-path-distillation-turnkey-system","title":"Neocision - 20L Neocision Dual Short Path Distillation Turnkey System","description":"\u003ch1\u003e20L Neocision Dual Short Path Distillation Turnkey System\u003c\/h1\u003e \u003cp\u003e\u003cspan\u003e\u003cem\u003eThis unit carries a 2 day lead time.\u003c\/em\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cdiv\u003e\u003cem\u003e(Note: This kit does NOT include the stainless steel table.)\u003c\/em\u003e\u003c\/div\u003e \u003cdiv\u003e\u003c\/div\u003e \u003cp\u003eThe 20L Neocision Distillation Turnkey Setup features our Dual \u003cspan\u003eUSA made\u003c\/span\u003e P10V6 Distillation Heads. Every component in this distillation kit is made for precision, throughput, and repeatable results. You will also receive Dual Dewar Style Ribbed Glass Cold Traps to keep all volatiles and solvents out of your vacuum system. \u003cspan\u003eThis Turnkey Setup gives you everything needed to perform distillation at the highest level.\u003c\/span\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cimg width=\"900\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/5\/assets\/description_image_distillationdiagramfinal_jpg?7355035109499693479\" alt=\"Distillation Flow Chart\" title=\"Distillation Flow Chart\"\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eThe 20L Neo Kit Includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e20L Neocision Kit with glassware, labware, and Dual P10V6 Distillation Heads.\u003c\/li\u003e \u003cli\u003eBVV 15 Liter Advanced Digital Heated Circulator\u003c\/li\u003e \u003cli\u003eChoice of Vacuum Pump \u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eKF-25 Bellow Y Manifold\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDual Ribbed Dewar Style Glass Cold Trap\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eNon-Mercury Glass Thermometers\u003c\/li\u003e \u003cli\u003e20L Digital Heating and Stirring Mantle\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in the boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003cli\u003eOnce process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003col\u003e\u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Note: This entire setup will ship via motor freight.***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e \u003cp\u003e\u003cspan\u003e*Notice to \u003c\/span\u003e\u003cspan\u003eCustomers\u003c\/span\u003e\u003cspan\u003e: All units are inspected for broken glassware or parts before leaving BVV. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer\u003c\/span\u003e\u003cspan\u003e \u003c\/span\u003e\u003cem\u003e\u003cstrong\u003eMUST contact BVV within 72 hours from carrier delivery to file a claim\u003c\/strong\u003e.\u003c\/em\u003e\u003cspan\u003e If the customer DOES NOT contact BVV within 72 hours from carrier delivery, then BVV cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. \u003c\/span\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cspan\u003eBVV is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.\u003c\/span\u003e\u003c\/p\u003e \u003cbr\u003e","brand":"BVV","offers":[{"title":"Bvv 21.2","offer_id":49567695733047,"sku":"20LNTK-21.2","price":13000.0,"currency_code":"USD","in_stock":true},{"title":"Bvv 21.2ul","offer_id":49567695765815,"sku":"20LNTK-21.2UL","price":14000.0,"currency_code":"USD","in_stock":true},{"title":"Edwards E2M28","offer_id":49567695798583,"sku":"20LNTK-E2M28","price":17000.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/585565ce8f223235ffbbf668bcac5a13.jpg?v=1758128141"},{"product_id":"20l-neocision-dual-head-short-path-distillation-kit","title":"Neocision - 20L Neocision Dual Head Short Path Distillation Kit","description":"\u003ch1\u003e20L Neocision Dual Head Short Path Distillation Kit\u003c\/h1\u003e \u003cp\u003e\u003cspan\u003e\u003cem\u003eThis unit carries a 2 day lead time.\u003c\/em\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cdiv\u003e\u003cem\u003e(Note: This kit does NOT include the stainless steel table.)\u003c\/em\u003e\u003c\/div\u003e \u003cdiv\u003e\u003c\/div\u003e \u003cp\u003eThe 20L Neocision Distillation Kit Setup features our Dual P10V6 Distillation Heads and USA made glass. Every component in this distillation kit is made for precision, throughput, and repeatable results. You will also receive Dual Dewar Style Ribbed Glass Cold Traps to keep all volatiles and solvents out of your vacuum system. This kit gives you the essentials of a short path distillation system and allows you to add a pump and temperature control system of your choosing.\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cimg title=\"Distillation Flow Chart\" alt=\"Distillation Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/5\/assets\/description_image_distillationdiagramfinal_jpg?7355035109499693479\" width=\"900\"\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eThe 20L Neo Kit Includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e20L Neocision Kit with glassware, labware, and Dual P10V6 Distillation Heads.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eKF-25 Bellow Y Manifold\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDual Ribbed Dewar Style Glass Cold Trap\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eNon-Mercury Glass Thermometers\u003c\/li\u003e \u003cli\u003e20L Digital Heating and Stirring Mantle\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in the boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003cli\u003eOnce process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003col\u003e\u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e*Note: This entire setup will ship via motor freight.***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cspan\u003e*Notice to \u003c\/span\u003e\u003cspan\u003eCustomers\u003c\/span\u003e\u003cspan\u003e: All units are inspected for broken glassware or parts before leaving BVV. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer\u003c\/span\u003e\u003cspan\u003e \u003c\/span\u003e\u003cem\u003e\u003cstrong\u003eMUST contact BVV within 72 hours from carrier delivery to file a claim\u003c\/strong\u003e.\u003c\/em\u003e\u003cspan\u003e If the customer DOES NOT contact BVV within 72 hours from carrier delivery, then BVV cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. \u003c\/span\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cspan\u003eBVV is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.\u003c\/span\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Non-Mercury Glass Thermometers","offer_id":49567697273143,"sku":"20LNKIT","price":12600.0,"currency_code":"USD","in_stock":true},{"title":"Digital Kangaroo Thermometer","offer_id":49567697305911,"sku":"20LNKIT-KANGAROO","price":12240.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/536ae271e0d6b1ff2adc81d89ff95f64.jpg?v=1758128100"},{"product_id":"10l-short-path-distillation-kit-with-p10-distillation-head","title":"BVV - 10L Premium Short Path Distillation Kit with P10 Distillation Head","description":"\u003ch1\u003e10L Short Path Distillation Kit with P10 Distillation Head\u003c\/h1\u003e \u003cp\u003e\u003cspan\u003e\u003cem\u003eThis unit carries\u003cspan\u003e \u003c\/span\u003ea 2 day lead time.\u003c\/em\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003e\u003cem\u003e(Note: Stainless Steel Table NOT Included.)\u003c\/em\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eThe 10L Short Path Distillation Kit features our USA made \u003cspan\u003eP10 Distillation Head.\u003c\/span\u003e Every component in this turnkey is made for precision, throughput, and repeatable results. Also included the Kangaroo digital thermometer which is very rugged and reliable. You will also receive a Ribbed Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Kit gives you the basic necessities of a short path distillation system and allows you to add on a temperature control system and vacuum pump to fit your needs.\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cimg title=\"Distillation Flow Chart\" alt=\"Distillation Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/5\/assets\/description_image_distillationdiagramfinal_jpg?7355035109499693479\" width=\"900\"\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eThe 10L Neo Kit Includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10L Short Path Distillation Kit including glassware, labware, and P10 Distillation Head.\u003c\/li\u003e \u003cli\u003e10L Digital Heating and Stirring Mantle.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eValved Vacuum Adapter.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRibbed Dewar Style Glass Cold Trap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eKangaroo Digital Thermometer.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003cli\u003eOnce process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003col\u003e\u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Note: This entire setup will ship via motor freight.***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cspan\u003e*Notice to \u003c\/span\u003e\u003cspan\u003eCustomers\u003c\/span\u003e\u003cspan\u003e: All units are inspected for broken glassware or parts before leaving BVV. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer\u003c\/span\u003e\u003cspan\u003e \u003c\/span\u003e\u003cem\u003e\u003cstrong\u003eMUST contact BVV within 72 hours from carrier delivery to file a claim\u003c\/strong\u003e.\u003c\/em\u003e\u003cspan\u003e If the customer DOES NOT contact BVV within 72 hours from carrier delivery, then BVV cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. \u003c\/span\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003eBVV is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.\u003c\/span\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e\u003cstrong\u003e\u003ciframe width=\"560\" height=\"315\" src=\"https:\/\/www.youtube.com\/embed\/Bi4sVnTv1S0\" frameborder=\"0\" allow=\"accelerometer; autoplay; encrypted-media; gyroscope; picture-in-picture\" allowfullscreen=\"\"\u003e\u003c\/iframe\u003e\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567698878775,"sku":"10LP10KIT","price":4100.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/4426c3d3ccd52800782dfe8cdec82a16.jpg?v=1758127977"},{"product_id":"10l-neocision-dual-head-short-path-distillation-kit","title":"Neocision - 10L Neocision Dual Head Short Path Distillation Kit","description":"\u003ch1\u003e10L Neocision Dual Head Short Path Distillation Kit\u003c\/h1\u003e \u003cdiv\u003e\u003cspan\u003e\u003cem\u003eThis unit carries a 2 day lead time.\u003c\/em\u003e\u003c\/span\u003e\u003c\/div\u003e \u003cbr\u003e \u003cp\u003eThe 10L Neocision Distillation Turnkey Setup features our Dual 10L P5 Distillation Heads and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market. You will also receive a Dual Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level.\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cimg title=\"Distillation Flow Chart\" alt=\"Distillation Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/5\/assets\/description_image_distillationdiagramfinal_jpg?7355035109499693479\" width=\"900\"\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eThe 10L Neo Kit Includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10L Neocision Kit with Dual P5 Distillation Heads\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eKF-25 90 Degree Long Manifold and Metering Valve\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDual Dewar Style Glass Cold Trap\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBullseye Precision Vacuum Gauge\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003cbr\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eOnce process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003cp\u003e\u003ciframe width=\"560\" height=\"315\" src=\"https:\/\/www.youtube.com\/embed\/QKmYVBUiLIg\" frameborder=\"0\" allow=\"accelerometer; autoplay; encrypted-media; gyroscope; picture-in-picture\" allowfullscreen=\"\"\u003e\u003c\/iframe\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Note: This entire setup will ship via motor freight.***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cspan\u003e*Notice to \u003c\/span\u003e\u003cspan\u003eCustomers\u003c\/span\u003e\u003cspan\u003e: All units are inspected for broken glassware or parts before leaving BVV. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer\u003c\/span\u003e\u003cspan\u003e \u003c\/span\u003e\u003cem\u003e\u003cstrong\u003eMUST contact BVV within 72 hours from carrier delivery to file a claim\u003c\/strong\u003e.\u003c\/em\u003e\u003cspan\u003e If the customer DOES NOT contact BVV within 72 hours from carrier delivery, then BVV cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. \u003c\/span\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cspan\u003eBVV is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.\u003c\/span\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567709528375,"sku":"10LNKIT","price":16560.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/c2c366a07c86572e529a38bba6b01d0f.jpg?v=1758127858"},{"product_id":"10l-neocision-dual-head-short-path-distillation-turnkey-system","title":"Neocision - 10L Neocision Dual Head Short Path Distillation Turnkey System","description":"\u003ch1\u003e10L Neocision Dual Head Short Path Distillation Turnkey System\u003c\/h1\u003e \u003cdiv\u003e\u003cspan\u003e\u003cem\u003eThis unit carries a 2 day lead time.\u003c\/em\u003e\u003c\/span\u003e\u003c\/div\u003e \u003cp\u003eThe 10L Neocision Distillation Turnkey Setup features our Dual 10L P5 Distillation Heads and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included is a KF-25 Vacuum Pump giving you extreme power and depth with a long lifespan, the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market, and a BVV 19L Heated Circulator for maximum condensation of vapors. You will also receive a Dual Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level.\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cimg title=\"Distillation Flow Chart\" alt=\"Distillation Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/5\/assets\/description_image_distillationdiagramfinal_jpg?7355035109499693479\" width=\"900\"\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eThe Premium Turnkey Kit Includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10L Neocision Kit with Dual P5 Distillation Heads\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eKF-25 2 Meter Bellows\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDual Dewar Style Glass Cold Trap\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBullseye Precision Vacuum Gauge\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003cspan\u003eBVV 19L Heated Circulator\u003c\/span\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eYour Choice Of KF-25 Vacuum Pump\u003cbr\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eOnce process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Note: This entire setup will ship via motor freight.***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV\u003cstrong\u003e is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Bvv 21.2","offer_id":49567714214199,"sku":"10LNTK-21.2","price":23850.0,"currency_code":"USD","in_stock":true},{"title":"Edwards E2M28","offer_id":49567714246967,"sku":"10LNTK-E2M28","price":31950.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/06980b2f75e6ee10a6582647dbab1cc9.jpg?v=1758127919"},{"product_id":"50l-bvv-triple-jacketed-glass-reactor","title":"BVV - 50L BVV Double Jacketed Glass Reactor","description":"\u003cp\u003eThe BVV Double Jacketed Glass Reactors are ideal for reaction applications involving extreme temperatures. They include an inner jacket for cooling or heating and an outer jacket for vacuum insulation. The outer jacket also alleviates moisture buildup so you can always see exactly what's happening inside the system.\u003c\/p\u003e \u003cp\u003eJacketed Reaction vessels are used for synthetic reaction of different types of materials in a controlled temperature and vacuum environment. Reaction Vessels can be used as an all in one tool for extraction, refinement, distillation, and homogenization. Consisting of an inner vessel with either one or two jackets, a reactor uses temperature differentials created by a chiller to change it's internal environment. Reaction vessels also operate under vacuum making them ideal for any atmospheric sensitive applications. They can be made out of glass or stainless steel and range in volume from 1L to 100L+.\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eTo run a reaction vessel most efficiently, you will need a chiller capable of bringing the internal temperature of the vessel to an extreme low, a chemical resistant vacuum pump, and a cold trap to catch any vapors that might pass through the condenser during operation. BVV Jacketed Reaction vessels are simple, cost-effective, and durable machines that allow you to process material quickly and efficiently.\u003c\/p\u003e \u003cul\u003e \u003cli\u003e\u003ca title=\"BVV Glass Reactor Diagram\" href=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/BVV_20L_and_50L_Glass_Reactor_Diagram.pptx?v=1640182330\" target=\"_blank\"\u003e\u003cstrong\u003eBVV 20L and 50L Glass Reactor Diagram\u003c\/strong\u003e\u003c\/a\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eSpecifications:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eGlass Material: GG-17 High Borosilicate Glass\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eInternal Volume: 50L\u003c\/li\u003e \u003cli\u003e10.5L Jacket Capacity\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eShelf Material: Aluminum Alloy\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eHomogenizer Power: 110V\/60Hz\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eHomogenizer Speed: 0-400 RPM\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDigital Homogenizer Control\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDigital temperature probe readout included\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDouble Jacket\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e3\/4\" Jacket Connections\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1\/4\" and 3\/8\" Vacuum Connections\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eLength: 24 in.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eWidth: 30 in.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eHeight: 90 in.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eDoes not include: \u003c\/strong\u003eChiller, Vacuum System, Cold Trap\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eRequires Assembly\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e\u003cb\u003e***Note:\u003c\/b\u003e All units are inspected for broken glass or parts before unit is shipped.\u003cb\u003e \u003c\/b\u003eIf unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer \u003cstrong\u003eMUST \u003c\/strong\u003econtact BVV \u003cstrong\u003ewithin 3 days\u003c\/strong\u003e \u003cstrong\u003eof delivery\u003c\/strong\u003e to file a claim and receive a replacement part. If customer \u003cstrong\u003eDOES NOT\u003c\/strong\u003e contact BVV \u003cstrong\u003ewithin 3 days of delivery\u003c\/strong\u003e responsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Disclaimer: This unit is intended for LEGAL purposes only, to be used in accordance with local laws and ordinances. Use only in WELL VENTILATED AREAS!***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: \u003cstrong\u003eBVV is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Without Condenser","offer_id":49567715230007,"sku":"50LTGR-V3","price":5000.0,"currency_code":"USD","in_stock":true},{"title":"With Condenser","offer_id":49567715262775,"sku":"50LTGR-V3-COND","price":5400.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/50l-bvv-double-jacketed-glass-reactor-817861.jpg?v=1726550003"},{"product_id":"20l-bvv-triple-jacketed-glass-reactor","title":"BVV - 20L BVV Double Jacketed Glass Reactor","description":"\u003cp\u003e \u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003eThe BVV Double Jacketed Glass Reactors are ideal for reaction applications involving extreme temperatures. They include an inner jacket for cooling or heating and an outer jacket for vacuum insulation. The outer jacket also alleviates moisture buildup so you can always see exactly what's happening inside the system.\u003c\/p\u003e \u003cp\u003eJacketed Reaction vessels are used for synthetic reaction of different types of materials in a controlled temperature and vacuum environment. Reaction Vessels can be used as an all in one tool for extraction, refinement, distillation, and homogenization. Consisting of an inner vessel with either one or two jackets, a reactor uses temperature differentials created by a chiller to change it's internal environment. Reaction vessels also operate under vacuum making them ideal for any atmospheric sensitive applications. They can be made out of glass or stainless steel and range in volume from 1L to 100L+.\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eTo run a reaction vessel most efficiently, you will need a chiller capable of bringing the internal temperature of the vessel to an extreme low, a chemical resistant vacuum pump, and a cold trap to catch any vapors that might pass through the condenser during operation. BVV Jacketed Reaction vessels are simple, cost-effective, and durable machines that allow you to process material quickly and efficiently.\u003c\/p\u003e \u003cul\u003e \u003cli\u003e\u003ca href=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/files\/BVV_20L_and_50L_Glass_Reactor_Diagram.pptx?v=1640182330\" title=\"BVV Glass Reactor Diagram\" target=\"_blank\"\u003e\u003cstrong\u003eBVV 20L and 50L Glass Reactor Diagram\u003c\/strong\u003e\u003c\/a\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eSpecifications:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eGlass Material: GG-17 High Borosilicate Glass\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eInternal Volume: 20L\u003c\/li\u003e \u003cli\u003e6.75L Jacket Capacity\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eShelf Material: Aluminum Alloy\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eHomogenizer Power: 110V\/60Hz\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eHomogenizer Speed: 0-400 RPM\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDigital Homogenizer Control\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDigital temperature probe readout included\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDouble Jacket\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e3\/4\" Jacket Connections\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1\/4\" and 3\/8\" Vacuum Connections\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eLength: 20 in.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eWidth: 30 in.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eHeight: 76 in.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eDoes not include: \u003c\/strong\u003eChiller, Vacuum System, Cold Trap\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eRequires Assembly\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e*Notice to\u003cspan\u003e \u003c\/span\u003ecustomers: All units are inspected for broken glassware or parts before\u003cspan\u003e \u003c\/span\u003eleaving BVV. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV within\u003cspan\u003e \u003c\/span\u003e72 hours from carrier delivery to file\u003cspan\u003e \u003c\/span\u003ea claim.\u003cspan\u003e \u003c\/span\u003eIf the customer DOES NOT contact BVV within 72 hours from carrier delivery, then BVV cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement.\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Disclaimer: This unit is intended for LEGAL purposes only, to be used in accordance with local laws and ordinances. Use only in WELL VENTILATED AREAS!***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: \u003cstrong\u003eBVV is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Without Condenser","offer_id":49567716639031,"sku":"20LTGR-V3","price":4500.0,"currency_code":"USD","in_stock":true},{"title":"With Condenser","offer_id":49567716671799,"sku":"20LTGR-V3-COND","price":4900.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/20l-bvv-double-jacketed-glass-reactor-499637.jpg?v=1726549816"},{"product_id":"2l-electric-rotary-evaporator-kit-with-bvv-water-circulation-vacuum-pump","title":"BVV - 2L Electric Rotary Evaporator Kit with BVV Water Circulation Vacuum Pump","description":"\u003ch1\u003e2L Electric Rotary Evaporator Kit with BVV Water Circulation Vacuum Pump\u003c\/h1\u003e \u003cbr\u003e \u003cp\u003e2L Electric Rotary Evaporator Kit with BVV Water Circulation Vacuum Pump setup includes all the neccessary components to successfully perform solvent recovery via rotary evaporation. A cold trap should always be used inline between your vacuum system and application to protect the pump from volatile vapors.\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cimg title=\"Rotovap Flow Chart\" alt=\"Rotovap Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/5\/assets\/description_image_rotovapflowchart_jpg?9687986143292858980\" width=\"900\"\u003e\u003c\/p\u003e \u003ciframe width=\"560\" height=\"315\" src=\"https:\/\/www.youtube.com\/embed\/dPBDK8GHZpg\" frameborder=\"0\" allow=\"accelerometer; autoplay; encrypted-media; gyroscope; picture-in-picture\" allowfullscreen=\"\"\u003e\u003c\/iframe\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e2L Rotary Evaporator Turnkey Setup includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003ca title=\"2L BVV Electric Lift Rotary Evaporator\" href=\"https:\/\/shopbvv.com\/products\/2l-best-value-electric-lift-rotary-evaporator\" target=\"_blank\"\u003e2L Electric Lift Rotary Evaporator\u003c\/a\u003e\u003c\/li\u003e \u003cul\u003e \u003cli\u003e90-day limited warranty \u003cspan\u003e(excludes glassware, consumables \u0026amp; moving parts)\u003c\/span\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003ca title=\"Water Circulation Vacuum Pump\" href=\"https:\/\/shopbvv.com\/products\/water-circulation-vacuum-pump\" target=\"_blank\"\u003eBVV Water Circulation Vacuum Pump\u003c\/a\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003ch3\u003e\u003cb\u003eRotovap Quick Start Guide\u003c\/b\u003e\u003c\/h3\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start \u003ca href=\"https:\/\/shopbvv.com\/blogs\/bvv-resources\/rotovap-basics\" title=\"Rotovap Basics\"\u003einstructions for rotovaps\u003c\/a\u003e. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs. \u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eClean and assemble unit. Make sure all pieces are cleaned and sterilized using an alcohol solution.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect chiller to the condenser and set to 0C (32F). Always fill a rotovap condenser from the top down (chiller output to top of the condenser, chiller input to bottom of the condenser).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect vacuum pump to cold trap and connect cold trap to the vacuum port on rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTurn on heat bath and set to 40C (113F).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce heat bath, chiller, and cold trap have reached desired temperatures, turn on the rotovap motor and set the speed to approximately 100 RPM (does not have to be precise). Keep in mind, higher RPM's will increase evaporation power but also increase heat load.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eStart vacuum pump and allow vacuum to pull down for a few minutes before injection.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce the vacuum has been pulled to a sufficient level (does not have to be precise but should be below 100 Torr), using the injection valve, very slowly inject approximately 500 mL of solution into evaporating flask and then close the valve. Allow this small amount to begin evaporating. You may see the chiller begin to rise in temperature, this is called \"priming\" the rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce the temperature stops rising or all liquid is almost completely evaporated, open the injection valve again very slowly so that a small amount of liquid begins to enter the evaporating flask. Do not close injection valve this time but continue to allow the solution to enter the evaporating flask.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAt this point, you must try to match the input speed to the output speed. What this means is that you should be injecting the same amount of liquid into the rotovap that is equal to the amount of liquid dripping from the condenser into the receiving flask. You will know that the input speed and output speed are matched because the chiller will remain at a stable temperature. If the chiller begins to rise, then you are injecting too much liquid. Dial back the valve until the chiller stabilizes.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce everything is stabilized, you may walk away from the rotovap if necessary. Check every so often to make sure temperatures remain stable and evaporation continues efficiently.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e \u003c\/p\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: \u003cstrong\u003eBVV is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567771033911,"sku":"RT2LE-BVVWCVP","price":1750.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/5dcc21fb475988ed2fc5b9e769ea1f75.jpg?v=1758126971"},{"product_id":"5l-neocision-short-path-distillation-turnkey-kit","title":"Neocision - 5L Neocision Short Path Distillation Turnkey Kit","description":"\u003ch2\u003e5L Neocision Short Path Distillation Turnkey Kit\u003c\/h2\u003e \u003cdiv\u003e\u003cspan\u003e\u003cem\u003eThis unit carries a 2 day lead time.\u003c\/em\u003e\u003c\/span\u003e\u003c\/div\u003e \u003cp\u003eThe 5L Premium Distillation Turnkey Setup features our 5L Distillation Kit with P5 Distillation Head and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included is our Pro Series Corrosion Resistant Two Stage Vacuum Pump giving you extreme power and depth with a long lifespan, the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market, and a BVV 19L Heated Circulator for maximum condensation of vapors. You will also receive a Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level.\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cimg title=\"Distillation Flow Chart\" alt=\"Distillation Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/5\/assets\/description_image_distillationdiagramfinal_jpg?7355035109499693479\" width=\"900\"\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eThe Premium Turnkey Kit Includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e5L Neocision Kit with P5 Distillation Head\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eKF-25 x 1\/4\" Barb Adapter\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDewar Style Glass Cold Trap\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBullseye Precision Vacuum Gauge\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBVV 19L MX Heated Circulator\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePro Series 21.2CFM Corrosion Resistant Two Stage Vacuum Pump \u003cspan\u003e \u003c\/span\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eOnce process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Note: This entire setup will ship via motor freight.***\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV\u003cstrong\u003e is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Bvv 21.2","offer_id":49567790891319,"sku":"5LNTK-21.2","price":18900.0,"currency_code":"USD","in_stock":true},{"title":"Edwards E2M28","offer_id":49567790924087,"sku":"5LNTK-E2M28","price":26550.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/7abb87300c020a2e6b0ab13147ae684b.jpg?v=1758128283"},{"product_id":"2l-premium-short-path-distillation-turnkey-setup-with-p2-distillation-head","title":"BVV - 2L Premium Short Path Distillation Turnkey Setup with P2 Distillation Head","description":"\u003ch1\u003e2L Premium Short Path Distillation Turnkey Setup with P2 Distillation Head\u003c\/h1\u003e \u003cbr\u003e \u003cp\u003eThe 2L Premium Distillation Turnkey Setup features our 2L Distillation Kit with P2 Distillation Head and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included is our Pro Series 11.3CFM Corrosion Resistant Two Stage Vacuum Pump giving you extreme power and depth with long lifespan, the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market, and a Polyscience 7L MX Heated Circulator for maximum condensation of vapors. You will also receive a Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level.\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cimg title=\"Distillation Flow Chart\" alt=\"Distillation Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_distillationdiagramfinal_jpg?17947351501589759142\" width=\"900\"\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eThe Premium Turnkey Kit Includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e2L Distillation Kit w\/ P2 Distillation Head\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eKF-25 x 1\/4\" Barb Adapter\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDewar Style Glass Cold Trap\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBullseye precision Vacuum Gauge\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePolyscience 7L MX Heated Circulator\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePro Series 14.1CFM Corrosion Resistant Two Stage Vacuum Pump\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003cli\u003eOnce the process is complete, stop heat, stop stir, and stop vacuum. Let the atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003col\u003e\u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Note: This entire setup will ship via motor freight.***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: \u003cstrong\u003eBVV is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Heated Circulator","offer_id":49567819530551,"sku":"2LP2TK-NEO7H","price":6000.0,"currency_code":"USD","in_stock":true},{"title":"Polyscience Heated Circulator","offer_id":49567819563319,"sku":"2LP2TK","price":7650.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/20baff6f3eb32019df45cb3df0bcb93e.jpg?v=1758128207"},{"product_id":"2l-standard-short-path-distillation-turnkey-setup","title":"BVV - 2L Standard Short Path Distillation Turnkey Setup","description":"\u003ch1\u003e2L Standard Short Path Distillation Turnkey Setup\u003c\/h1\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003eThe Standard Distillation Turnkey Setup includes all the components necessary to successfully perform distillation at an entry-level price point.\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cem\u003eCrossbar pictured is not included. We recommend purchasing multiple lab stands to accommodate your specific needs. \u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003e\u003cimg width=\"900\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_distillationdiagramfinal_jpg?6704654464148641207\" alt=\"Distillation Flow Chart\" title=\"Distillation Flow Chart\"\u003e\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eThe Standard Turnkey Setup Includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003ca href=\"https:\/\/shopbvv.com\/products\/2l-distillation-kit\" target=\"_blank\"\u003e2L Distillation Kit\u003c\/a\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1\/4\" Flare x 1\/4\" Barb Adapter\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003ca title=\"BVV 5L\" href=\"https:\/\/shopbvv.com\/products\/bvv-5l-heated-circulator\" target=\"_blank\"\u003eBVV 5L Heated Circulator\u003c\/a\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBVV V9D 9CFM Two Stage Vacuum Pump\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e \u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003cspan\u003eHigh quality and durable Borosilicate 3.3 glass\u003c\/span\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e \u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003cspan\u003eVacuum-jacketed distillation adapter\u003c\/span\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e \u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003cspan\u003e3-way cow adapter, accommodating up to 3 pcs of 500mL flasks\u003c\/span\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e \u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003cspan\u003eGCT-01 cold trap guarding from damage of vapors\u003c\/span\u003e\u003c\/li\u003e \u003cli\u003e\u003cspan\u003eKangaroo Traceable Digital Thermometer\u003c\/span\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e \u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003cspan\u003eFlexible Gum Rubber Vacuum Tubing and Silicone Tubing for Flow\u003c\/span\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. The pump should be run against the dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003cli\u003eOnce the process is complete, stop heat, stop stir, and stop vacuum. Let the atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003col\u003e\u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Note: This entire setup will ship via motor freight.***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e \u003cp\u003e\u003cspan\u003e*Notice to \u003c\/span\u003e\u003cspan\u003eCustomers\u003c\/span\u003e\u003cspan\u003e: All units are inspected for broken glassware or parts before leaving BVV. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer\u003c\/span\u003e\u003cspan\u003e \u003c\/span\u003e\u003cem\u003e\u003cstrong\u003eMUST contact BVV within 72 hours from carrier delivery to file a claim\u003c\/strong\u003e.\u003c\/em\u003e\u003cspan\u003e If the customer DOES NOT contact BVV within 72 hours from carrier delivery, then BVV cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. \u003c\/span\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cspan\u003eBVV is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.\u003c\/span\u003e\u003c\/p\u003e \u003cbr\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567820546359,"sku":"2LTK","price":2600.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/a1846bb80fe5e1a4b6be002b9a2ea137.jpg?v=1758128237"},{"product_id":"2l-distillation-kit-with-p2-distillation-head","title":"BVV - 2L Short Path Distillation Kit with P2 Distillation Head","description":"\u003ch1\u003e2L Short Path Distillation Kit with P2 Distillation Head\u003c\/h1\u003e \u003cbr\u003e \u003cp\u003e \u003c\/p\u003e \u003cbr\u003e \u003cp\u003eThe 2L Distillation Kit w\/ P2 Distillation Head includes everything needed to perform distillation excluding the vacuum pump and chiller. This kit features our USA made P2 Distillation Head as well as USA made glass. It is designed with ease of use in mind and includes the highest quality components to ensure results are repeatable time and again. \u003cem\u003e\u003cbr\u003e\u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cem\u003e**This Kit Does NOT include a vacuum pump or circulator. Please see the below recommendations for both as well as recommended add-ons. Or check out our 2L Premium Turnkey Setup which includes vacuum pump and circulator.**\u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cem\u003eCrossbar pictured is not included. We recommend purchasing multiple lab stands to accomodate your specific needs. \u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eRecommended Vacuum Pumps: \u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePro Series 5.6CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eJust Better 6 CFM 2 Stage Deep Vacuum Pump (USA made economy option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eWelch 1400 DuoSeal 0.9 cfm 0.1 Micron Belt Drive Dual-Stage Pump\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003eRecommended Circulators:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePolyscience 7 Liter MX Heated Circulator (economy option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePolyscience 7 Liter MX Refrigerated Circulator (premium option with chilling capability)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003eRecommended Add-Ons: \u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eGlass Dewar Style Cold Trap (recommended cold trap)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBullseye Precison Vacuum Gauge (premium vacuum gauge for measuring depth)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eCT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eJ-KEM Digital Vapor Temp Monitor (digital vapor temp monitor with data-logging capabilities)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003eSpecifications:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBoiling Flask Size: 2L\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eReceveiving Flask Size: 250mL\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBatch Capacity approximate: 2L = 400-1000 grams\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRun time: 4 to 8 hours dependent upon material composition and throughput\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDistillation Temperature Range: 140-250C (Do not exceed 250C)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRecommended Condenser Temperature: 40-50C\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003eThis Kit Includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cem\u003eGlass components:\u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e2L USA Made 2-Neck Boiling Flask\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eP2 USA Made Distillation Head\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTriple Neck Cow\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e3x 250mL Receiving Flask\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e2x 24\/40 Chemglass Thermometer Inlet Adapter\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e120mm Glass Funnel\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cem\u003eAccessories:\u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eMagnetic PTFE Stirring Bar Retriever\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e5 Pack of Metal Keck Clips\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDow Corning High Vacuum Silicone Grease\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTripod Stand\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e2L Digital Heating and Stirring Mantle\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e3 Finger Clamp Adjustable 0-70mm\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e6\" x 6\" Scissor Jack\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e250-500ml Cork Stand\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10ft of Vacuum Hose\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10ft of Chiller Hose\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1\/4\" Vacuum Manifold\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTraceable Kangaroo Thermometer - Digital\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10 Pack of Adjustable Stainless Steel Tubing Clamps\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eFiberglass Insulation Rope 10 Feet\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w\/ 2x 1\/4\" Barb Adapters\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eOnce process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cspan\u003e*Notice to \u003c\/span\u003e\u003cspan\u003eCustomers\u003c\/span\u003e\u003cspan\u003e: All units are inspected for broken glassware or parts before leaving BVV. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer\u003c\/span\u003e\u003cspan\u003e \u003c\/span\u003e\u003cem\u003e\u003cstrong\u003eMUST contact BVV within 72 hours from carrier delivery to file a claim\u003c\/strong\u003e.\u003c\/em\u003e\u003cspan\u003e If the customer DOES NOT contact BVV within 72 hours from carrier delivery, then BVV cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. \u003c\/span\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cspan\u003eBVV is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.\u003c\/span\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567821103415,"sku":"2LP2DK","price":2200.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/2l-short-path-distillation-kit-with-p2-distillation-head-301144.jpg?v=1726549946"},{"product_id":"2l-distillation-kit","title":"BVV - 2L Short Path Distillation Kit","description":"\u003ch2\u003eShort Path Distillation Setup\u003c\/h2\u003e \u003cbr\u003e \u003cp\u003e\u003cimg title=\"Distillation Flow Chart\" alt=\"Distillation Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_distillationdiagramfinal_jpg?632197998369606337\" width=\"900\"\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003e\u003ciframe width=\"560\" height=\"315\" src=\"https:\/\/www.youtube.com\/embed\/U6A7zofqvWo\" frameborder=\"0\" allow=\"accelerometer; autoplay; encrypted-media; gyroscope; picture-in-picture\" allowfullscreen=\"\"\u003e\u003c\/iframe\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003eShort path distillation is used for compounds that are not stable at high temperatures. It can also be used to purify small amounts of a compound.\u003c\/span\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cspan\u003eFor those new to this type of distillation, our Short Path Kit includes everything you will need as you get started. All stands, clamps, clips, and tubing are included, which means it's ready to start working straight out of the box. \u003c\/span\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cspan\u003eThe cold trap, cow and vacuum grease can all be customized to meet your needs.\u003c\/span\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eThe 2L Distillation Kit builds upon the same principal as the 1L Distillation Kit, giving users an easy to use system that will get them up and running at an affordable price. It includes all stands, clamps, clips, and tubing needed to begin distilling immediately.\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cem\u003eThis Kit Does NOT include a vacuum pump or circulator. Please see the below recommendations for both as well as recommended add-ons. Or check out our \u003ca title=\"2L Standard Short Path Distillation Turnkey Setup\" href=\"https:\/\/shopbvv.com\/products\/2l-standard-short-path-distillation-turnkey-setup\"\u003e2L Standard Distillation Turnkey Setup\u003c\/a\u003e which includes vacuum pump and circulator. \u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cem\u003eCrossbar pictured is not included. We recommend purchasing multiple lab stands to accommodate your specific needs. \u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e \u003ch3\u003e\u003cstrong\u003eRecommended Vacuum Pumps: \u003c\/strong\u003e\u003c\/h3\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePro Series 5.6CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eJust Better 6 CFM 2 Stage Deep Vacuum Pump (economy option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBest Value Vacs VE280 9CFM Two Stage Vacuum Pump (economy option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003ch3\u003e\u003cstrong\u003eRecommended Circulators:\u003c\/strong\u003e\u003c\/h3\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePolyscience 7 Liter MX Heated Circulator (economy option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePolyscience 7 Liter MX Refrigerated Circulator (premium option with chilling capability)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003ch3\u003e\u003cstrong\u003eRecommended Add-Ons: \u003c\/strong\u003e\u003c\/h3\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eGlass Dewar Style Cold Trap (recommended cold trap)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBullseye Precison Vacuum Gauge (premium vacuum gauge for measuring depth)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eCT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003ch2\u003e\u003cstrong\u003eShort Path Distillation Kit Specifications:\u003c\/strong\u003e\u003c\/h2\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBoiling Flask Size: 2L\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRecieving Flask Size: 250ml\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBatch Capacity approximate: 2L = 400-1000 grams\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRun time: 4 to 8 hours dependent upon material composition and throughput\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDistillation Temperature Range: 140-250C (Do not exceed 250C)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRecommended Condenser Temperature: 40-50C\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003ch3\u003e\u003cstrong\u003eThis Kit Comes Standard With The Following:\u003c\/strong\u003e\u003c\/h3\u003e \u003cp\u003e\u003cem\u003eGlass Components:\u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e2L 2-Neck Boiling Flask\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eShort Path Head\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTriple Neck Cow\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e3x 250mL Single Neck Receiving Flask\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1\/8\" 14\/20 PTFE Thermometer Adapter\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1\/4\" 24\/40 PTFE Thermometer Adapter\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e120mm Glass Funnel\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cem\u003eAccessories:\u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eMagnetic PTFE Stirring Bar Retriever\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e5 Pack of Metal Keck Clips\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDow Corning High Vacuum Silicone Grease\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTripod Stand\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e2L Digital Heating and Stirring Mantle\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e3 Finger Clamp Adjustable 0-70mm\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e6\" x 6\" Scissor Jack\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e250-500ml Cork Stand\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10ft of Vacuum Hose\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10ft of Chiller Hose\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1\/4\" Vacuum Manifold\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTraceable Kangaroo Thermometer - Digital\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10 Pack of Adjustable Stainless Steel Tubing Clamps\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eFiberglass Insulation Rope 10 Feet\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w\/ 2x 1\/4\" Barb Adapters\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003ch2\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/h2\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs.\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e \u003ca title=\"Vacuum Pumps\" href=\"https:\/\/shopbvv.com\/collections\/vacuum-pumps\"\u003eVacuum Pump\u003c\/a\u003e is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003cli\u003eOnce process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e \u003c\/p\u003e \u003cp\u003eLearn more about short path distillation components and FAQs with \u003ca title=\"Short Path Distillation Guide\" href=\"https:\/\/shopbvv.com\/blogs\/bvv-resources\/short-path-distillation-basics\"\u003ethis distillation guide\u003c\/a\u003e.\u003cbr\u003e\u003c\/p\u003e \u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cspan\u003e*Notice to \u003c\/span\u003e\u003cspan\u003eCustomers\u003c\/span\u003e\u003cspan\u003e: All units are inspected for broken glassware or parts before leaving BVV. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer\u003c\/span\u003e\u003cspan\u003e \u003c\/span\u003e\u003cem\u003e\u003cstrong\u003eMUST contact BVV within 72 hours from carrier delivery to file a claim\u003c\/strong\u003e.\u003c\/em\u003e\u003cspan\u003e If the customer DOES NOT contact BVV within 72 hours from carrier delivery, then BVV cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. \u003c\/span\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cspan\u003eBVV is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.\u003c\/span\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567821889847,"sku":"2LDK","price":1275.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/2l-short-path-distillation-kit-101774.jpg?v=1726549947"},{"product_id":"5l-premium-distillation-turnkey-setup","title":"BVV - 5L Premium Short Path Distillation Turnkey Setup","description":"\u003ch1\u003e5L Premium Distillation Kit\u003c\/h1\u003e \u003cdiv\u003e\u003cspan\u003e\u003cem\u003eThis unit carries a 2 day lead time.\u003c\/em\u003e\u003c\/span\u003e\u003c\/div\u003e \u003cp\u003eThe 5L Premium Short Path Distillation Turnkey Setup features our 5L Distillation Kit with P5 Distillation Head and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included is our Pro Series 11.3CFM Corrosion Resistant Two Stage Vacuum Pump giving you extreme power and depth with a long lifespan, the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market, and a BVV 19L Heated Circulator for maximum condensation of vapors. You will also receive a Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level.\u003c\/p\u003e \u003cbr\u003e \u003cdiv\u003e\u003cimg alt=\"Short Path Distillation Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_distillationdiagramfinal_jpg?16584312337360568117\"\u003e\u003c\/div\u003e \u003cbr\u003e \u003ch3\u003e\u003cstrong\u003eThe Premium Short Path Distillation Turnkey Kit Includes:\u003c\/strong\u003e\u003c\/h3\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003ca href=\"https:\/\/shopbvv.com\/products\/5l-short-path-distillation-kit-with-p5-distillation-head\" title=\"5L Distillation Kit\" target=\"_blank\"\u003e5L Distillation Kit with P5 Distillation Head \u003c\/a\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eKF-25 x 1\/4\" Barb Adapter\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDewar Style Glass Cold Trap\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBullseye Precision Vacuum Gauge\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePolyscience 7L MX Heated Circulator\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePro Series 14.1CFM Corrosion Resistant Two Stage Vacuum Pump \u003cspan\u003e \u003c\/span\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e \u003c\/p\u003e \u003ch3\u003e\u003cb\u003eShort Path Distillation Quick Start Guide\u003c\/b\u003e\u003c\/h3\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003eOnce all three of these steps have been completed, you are \u003ca href=\"https:\/\/shopbvv.com\/blogs\/bvv-resources\/short-path-distillation-basics\" title=\"Basic Guide To Short Path Distillation\"\u003eready to begin distilling\u003c\/a\u003e.\u003c\/p\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003cli\u003eOnce the process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003col\u003e\u003c\/ol\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Note: This entire setup will ship via motor freight.***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003chr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV\u003cstrong\u003e is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567823298871,"sku":"5LP5TK","price":9900.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/78566a16878b2c3d22706ca1be74cc64.jpg?v=1758128341"},{"product_id":"5l-short-path-distillation-kit-with-p5-distillation-head","title":"BVV - 5L Short Path Distillation Kit with P5 Distillation Head","description":"\u003ch2\u003e5L Short Path Distillation Kit with P5 Distillation Head\u003c\/h2\u003e \u003cdiv\u003e\u003cspan\u003e\u003cem\u003eThis unit carries a 2 day lead time.\u003c\/em\u003e\u003c\/span\u003e\u003c\/div\u003e \u003cp\u003e\u003cimg width=\"900\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_distillationdiagramfinal_jpg?16869437120855438583\" alt=\"Distillation Flow Chart\" title=\"Distillation Flow Chart\"\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003eThe 5L Distillation Kit includes everything needed to perform distillation excluding the vacuum pump and chiller. This kit features our USA made P5 Distillation Head, as well as USA, made glass. This Kit is designed for high volume production with the highest quality components for precise, repeatable results time and again.\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cem\u003eThis Kit Does NOT include a vacuum pump or chiller. Please see the below recommendations for both as well as recommended add-ons.\u003c\/em\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eRecommended Vacuum Pumps:\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePro Series 11.3CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eJust Better 6 CFM 2 Stage Deep Vacuum Pump (economy option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eRecommended Chillers:\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePolyscience 7 Liter MX Heated Circulator (economy option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePolyscience 7 Liter Refrigerated Circulator (premium option with chilling capability)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eRecommended Add-Ons:\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eGlass Dewar Style Cold Trap (recommended cold trap)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBullseye Precision Vacuum Gauge (premium vacuum gauge for measuing depth)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eCT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eJ-KEM Digital Vapor Temp Monitor (digital vapor temp monitor with data-logging capabilites)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eSpecifications:\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBoiling Flask Size: 5L\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eReceiving Flask Size: 2x 500mL, 1000mL\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBatch Capacity approximate: 1000-2500 grams\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRun time: 4 to 8 hours dependent upon material composition and throughput\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDistillation Temperature Range: 140-250C (Do not exceed 250C)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRecommended Condenser Temperature: 40-50C\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eThis Kit Includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cem\u003eGlass components:\u003c\/em\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e5L Boiling Flask\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eP5V6 Distillation Head\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTriple Neck Cow\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e2x 500mL Receiving Flask\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1L Receiving Flask\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e120mm Glass Funnel\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cem\u003eAccessories:\u003c\/em\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePTFE Magnetic Stir Bar Retriever\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e5 Pack of Metal Keck Clips\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDow Corning High Vacuum Silicone Grease\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTripod Stand\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e5L Digital Heating and Stirring Mantle\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e3-Finger Adjustable Clamp 0-77mm\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e6\" x 6\" Scissor Jack\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e500-1000mL Cork Stand\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e2x 24\/40 ChemglassPTFE Thermometer Inlet Adapter\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10ft of Gum Rubber Vacuum Hose\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10ft of Silicone Chiller Hose\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1\/4\" Vacuum Manifold\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTraceable Kangaroo Thermometer - Digital\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10 Pack of Adjustable Stainless Steel Tubing Clamps\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eFiberglass Insulation Rope 10 Feet\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w\/ 2x 1\/4\" Barb Adapters\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003col\u003e \u003col\u003e \u003cli\u003eOnce process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cspan\u003e*Notice to \u003c\/span\u003e\u003cspan\u003eCustomers\u003c\/span\u003e\u003cspan\u003e: All units are inspected for broken glassware or parts before leaving BVV. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer\u003c\/span\u003e\u003cspan\u003e \u003c\/span\u003e\u003cem\u003e\u003cstrong\u003eMUST contact BVV within 72 hours from carrier delivery to file a claim\u003c\/strong\u003e.\u003c\/em\u003e\u003cspan\u003e If the customer DOES NOT contact BVV within 72 hours from carrier delivery, then BVV cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. \u003c\/span\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cspan\u003eBVV is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.\u003c\/span\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567824412983,"sku":"5LP5KIT","price":3960.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/5l-short-path-distillation-kit-with-p5-distillation-head-968369.jpg?v=1726549966"},{"product_id":"1l-distillation-kit","title":"BVV - 1L Distillation Kit","description":"\u003ch1\u003e1L Distillation Kit\u003c\/h1\u003e \u003cbr\u003e \u003cp\u003e\u003cimg width=\"900\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_distillationdiagramfinal_jpg?7009835877274140877\" alt=\"Distillation Flow Chart\" title=\"Distillation Flow Chart\"\u003e\u003c\/p\u003e \u003cp\u003eThe 1L Distillation Kit is a simple, easy to use system designed for small personal use. It includes all stands, clamps, clips, and tubing needed to begin distilling immediately. \u003cem\u003e\u003cbr\u003e\u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cem\u003eThis Kit Does NOT include a vacuum pump or circulator. Please see the below recommendations for both as well as recommended add-ons. Or check out our 1L Standard Distillation Turnkey Setup which includes vacuum pump and circulator. \u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eRecommended Vacuum Pumps: \u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePro Series 5.6CFM Corrosion Resistant Two Stage Vacuum Pump (premium option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eJust Better 6 CFM 2 Stage Deep Vacuum Pump (USA made economy option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBest Value Vacs VE280 9CFM \u003ca title=\"BVV V9D 9CFM Two Stage Vacuum Pump\" href=\"https:\/\/shopbvv.com\/collections\/best-value-vacs-ve-series\/products\/bvv-trade-v9d-9cfm-two-stage-vacuum-pump\"\u003eTwo Stage Vacuum Pump\u003c\/a\u003e (economy option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003eRecommended Circulator:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePolyscience 7 Liter MX Heated Circulator (economy option)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003ePolyscience 7 Liter MX Refrigerated Circulator (premium option with chilling capability)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003eRecommended Add-Ons: \u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eGlass Dewar Style Cold Trap (recommended cold trap)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBullseye Precison Vacuum Gauge (premium vacuum gauge for measuring depth)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eCT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003eSpecifications:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBoiling Flask Size: 1L\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eReceveiving Flask Size: 250ml\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBatch Capacity approximate: 200-400 grams\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRun time: 4 to 8 hours dependent upon material composition and throughput\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDistillation Temperature Range: 140-250C (Do not exceed 250C)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eRecommended Condenser Temperature: 40-50C\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cstrong\u003eThis Kit Includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cem\u003eGlass Components:\u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1L 2-Neck Boiling Flask\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eShort Path Head\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTriple Neck Cow Receiving Flask\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e3x 250ml Single Neck Round Bottom Flask\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e14\/20 Thermometer Adapter\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e24\/40 Thermometer Adapter\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e120mm Glass Funnel\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e14\/20 Stopper\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e24\/40 Stopper\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cem\u003eAccessories: \u003c\/em\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eMagnetic PTFE Stirring Bar Retriever\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e5 Pack of Metal Keck Clips\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eDow Corning High Vacuum Silicone Grease\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTripod Stand\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1L Analog Heating and Stirring Mantle\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e3 Finger Clamp Adjustable 0-70mm\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBoss Head -13mm\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e6\" x 6\" Scissor Jack\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e250-500ml Cork Stand\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10ft of Vacuum Hose\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10ft of Chiller Hose\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1\/4\" Vacuum Manifold\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTraceable Kangaroo Thermometer - Digital\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10 Pack of Adjustable Stainless Steel Tubing Clamps\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eFiberglass Insulation Rope 10 Feet\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w\/ 2x 1\/4\" Barb Adapters\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e\u003cbr\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003col\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003cli\u003eOnce process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003c\/ol\u003e \u003cbr\u003e\u003chr\u003e \u003cp\u003e\u003cspan\u003e*Notice to \u003c\/span\u003e\u003cspan\u003eCustomers\u003c\/span\u003e\u003cspan\u003e: All units are inspected for broken glassware or parts before leaving BVV. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer\u003c\/span\u003e\u003cspan\u003e \u003c\/span\u003e\u003cem\u003e\u003cstrong\u003eMUST contact BVV within 72 hours from carrier delivery to file a claim\u003c\/strong\u003e.\u003c\/em\u003e\u003cspan\u003e If the customer DOES NOT contact BVV within 72 hours from carrier delivery, then BVV cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. \u003c\/span\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cspan\u003eBVV is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.\u003c\/span\u003e\u003c\/p\u003e \u003cbr\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567858426167,"sku":"1LDK","price":900.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/1l-distillation-kit-616731.jpg?v=1726549812"},{"product_id":"fiberglass-insulation-rope-10-feet","title":"BVV - Fiberglass Insulation Rope 10 Feet","description":"\u003ch1\u003eFiberglass Insulation Rope 10 Feet\u003c\/h1\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003e***Caution: Always use proper protection when working with fiberglass. Avoid skin and eye contact.***\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e \u003cp\u003eTen feet of white 1\/2\" fiberglass insulation rope. Used to wrap the upper half of boiling flasks.\u003c\/p\u003e \u003cbr\u003e \u003cp\u003e\u003cstrong\u003eSpecifications:\u003c\/strong\u003e\u003c\/p\u003e \u003cbr\u003e\u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eWidth: 1\/2\"\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eMaterial: Fiberglass\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eMaximum Temperature: 1000F\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eResistant to solvents, acids, and bleach\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eColor: White\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cbr\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eLength: 10 ft. (20ft needed for 5L Flask.)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e","brand":"BVV","offers":[{"title":"Default Title","offer_id":49567869993271,"sku":"FIR10","price":28.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/fiberglass-insulation-rope-10-feet-764929.jpg?v=1726551136"},{"product_id":"2l-rotary-evaporator-turnkey-setup","title":"BVV - 2L BVV Rotary Evaporator Turnkey Setup","description":"\u003ch1\u003e2L BVV Rotary Evaporator Turnkey Setup\u003c\/h1\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e2L Electric Lift Rotary Evaporator turnkey setup includes all the necessary components to successfully perform solvent recovery via rotary evaporation. A cold trap should always be used inline between your vacuum system and application to protect the pump from volatile vapors.\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cimg title=\"Rotovap Flow Chart\" alt=\"Rotovap Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_rotovapflowchart_jpg?130795633027647600\" width=\"900\"\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e2L Rotary Evaporator Turnkey Setup includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003ca href=\"https:\/\/shopbvv.com\/products\/2l-best-value-electric-lift-rotary-evaporator\" title=\"2L BVV Electric Lift Rotary Evaporator\"\u003e2L Electric Lift Rotary Evaporator\u003c\/a\u003e\u003c\/li\u003e \u003cul\u003e \u003cli\u003e90-day limited warranty (excludes glassware, consumables \u0026amp; moving parts)\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e \u003ca title=\"NEO 1.4CFM Diaphragm Pump ETL Rated\" href=\"https:\/\/shopbvv.com\/products\/neo-diaphragm-pump-etl-rated\"\u003eBVV NEO 1.4 CFM Diaphragm Pump ETL Rated\u003c\/a\u003e OR. \u003cspan\u003e3.5CFM Dry Floating Scroll Vacuum Pump\u003c\/span\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e \u003ca title=\"Polyscience LS 1\/2HP Chiller, Turbine Pump\" href=\"https:\/\/shopbvv.com\/products\/polyscience-ls-20c-to-40c-1-2hp-chiller-w-turbine-pump\"\u003ePolyscience LS -20C to 40C 1\/2HP Chiller w\/ Turbine Pump\u003c\/a\u003e OR \u003ca title=\"NEOCISION 20L Chiller (-40c) - ETL Rated\" href=\"https:\/\/shopbvv.com\/products\/neocision-20l-chiller-40c-etl-rated\"\u003eBVV NEOCISION 20L Chiller (-40C) - ETL Rated\u003c\/a\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10ft of Vacuum Tubing\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e20ft of Chiller Tubing\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e10 Pack of Adjustable stainless steel hose clamps\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e3\/8\" Vacuum Manifold\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOptional add-on : \u003cspan\u003eBVV CT40 -40degF 300ml x 3 Cold Trap, \u003cspan\u003eBVV CT80 -112degF 300ml x 3 Cold Trap\u003c\/span\u003e\u003c\/span\u003e\u003ca title=\"CT80\" href=\"BVV%20CT80%20-112%C2%B0F%20300ml%20x%203%20Cold%20Trap\" target=\"_blank\"\u003e \u003c\/a\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOptional add-on: J-KEM DVR-200 Digital Vacuum Regulator\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOptional add-on: Heat Transfer Fluid -- NuTherm PF-50 or Dynalene HC-50\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eRotovap Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start \u003ca title=\"Rotovap Basics\" href=\"https:\/\/shopbvv.com\/blogs\/bvv-resources\/rotovap-basics\"\u003einstructions for rotovaps\u003c\/a\u003e. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs. \u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eClean and assemble unit. Make sure all pieces are cleaned and sterilized using an alcohol solution.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect chiller to the condenser and set to 0C (32F). Always fill a rotovap condenser from the top down (chiller output to top of the condenser, chiller input to bottom of the condenser).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eConnect vacuum pump to cold trap and connect cold trap to the vacuum port on rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eTurn on heat bath and set to 40C (113F).\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce heat bath, chiller, and cold trap have reached desired temperatures, turn on the rotovap motor and set the speed to approximately 100 RPM (does not have to be precise). Keep in mind, higher RPM's will increase evaporation power but also increase heat load.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eStart vacuum pump and allow vacuum to pull down for a few minutes before injection.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce the vacuum has been pulled to a sufficient level (does not have to be precise but should be below 100 Torr), using the injection valve, very slowly inject approximately 500 mL of solution into evaporating flask and then close the valve. Allow this small amount to begin evaporating. You may see the chiller begin to rise in temperature, this is called \"priming\" the rotovap.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce the temperature stops rising or all liquid is almost completely evaporated, open the injection valve again very slowly so that a small amount of liquid begins to enter the evaporating flask. Do not close injection valve this time but continue to allow the solution to enter the evaporating flask.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAt this point, you must try to match the input speed to the output speed. What this means is that you should be injecting the same amount of liquid into the rotovap that is equal to the amount of liquid dripping from the condenser into the receiving flask. You will know that the input speed and output speed are matched because the chiller will remain at a stable temperature. If the chiller begins to rise, then you are injecting too much liquid. Dial back the valve until the chiller stabilizes.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eOnce everything is stabilized, you may walk away from the rotovap if necessary. Check every so often to make sure temperatures remain stable and evaporation continues efficiently.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV\u003cstrong\u003e is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"NEO 20 L Chiller \/ NEO 1.4CFM Diaphragm Pump ETL RATED \/ NEO 1.4CFM Diaphragm Pump ETL RATED","offer_id":49567876940087,"sku":"2LRETS-NEO","price":14000.0,"currency_code":"USD","in_stock":true},{"title":"NEO 20 L Chiller \/ Scroll Pump (Non-Certified) \/ Scroll Pump (Non-Certified)","offer_id":49567876972855,"sku":"2LRETS-2-NONEUL-2","price":14000.0,"currency_code":"USD","in_stock":true},{"title":"Polyscience 1\/2HP Chiller \/ NEO 1.4CFM Diaphragm Pump ETL RATED \/ NEO 1.4CFM Diaphragm Pump ETL RATED","offer_id":49567876874551,"sku":"2LRETS-2","price":27000.0,"currency_code":"USD","in_stock":true},{"title":"Polyscience 1\/2HP Chiller \/ Scroll Pump (Non-Certified) \/ Scroll Pump (Non-Certified)","offer_id":49567876907319,"sku":"2LRETS-2-NONEUL","price":27000.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/842ed27cddd75cf03e06b7165d03a3ff.jpg?v=1758126967"},{"product_id":"1l-standard-distillation-turnkey-setup","title":"BVV - 1L Standard Distillation Turnkey Setup","description":"\u003ch2\u003e1L Standard Distillation Turnkey Setup \u003c\/h2\u003e \u003cp\u003eThe Standard Distillation Turnkey Setup includes all the components necessary to successfully perform distillation at an entry level price point.\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e\u003cimg title=\"Distillation Flow Chart\" alt=\"Distillation Flow Chart\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_distillationdiagramfinal_jpg?9268547186388993654\" width=\"900\"\u003e\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003eThe Standard Turnkey Setup Includes:\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003ca href=\"https:\/\/shopbvv.com\/products\/1l-distillation-kit\" title=\"1L Kit\" target=\"_blank\"\u003e1L Distillation Kit\u003c\/a\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e1\/4\" Flare x 1\/4\" Barb Adapter\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003e\u003ca href=\"https:\/\/shopbvv.com\/products\/bvv-5l-heated-circulator\" target=\"_blank\"\u003eBVV 5L Heated Circulator\u003c\/a\u003e\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eBVV V9D 9CFM Two Stage Vacuum Pump\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eDistillation Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs,\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003eBefore beginning distillation, ensure the following steps have been taken:\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eVacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed.\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eAll glass components are in good working order and ready to be assembled\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cul\u003e \u003cli\u003eA winterization and degassing procedure has been done to prepare oil for distillation\u003c\/li\u003e \u003c\/ul\u003e \u003c\/ul\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003eOnce all three of these steps have been completed, you are ready to begin distilling.\u003c\/p\u003e \u003col\u003e \u003cli\u003eBegin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer.\u003c\/li\u003e \u003cli\u003eAssemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware\u003c\/li\u003e \u003cli\u003eAttach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation.\u003c\/li\u003e \u003cli\u003eConnect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system.\u003c\/li\u003e \u003cli\u003eConnect receiving cow to cold trap.\u003c\/li\u003e \u003cli\u003eConnect cold trap to manifold.\u003c\/li\u003e \u003cli\u003eConnect vacuum gauge to manifold.\u003c\/li\u003e \u003cli\u003eAt this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process.\u003c\/li\u003e \u003cli\u003eTurn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability.\u003c\/li\u003e \u003cli\u003eStart stir slower and increase speed with temperature.\u003c\/li\u003e \u003cli\u003eOnce you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C.\u003c\/li\u003e \u003cli\u003eYou will see your first fraction somewhere between 180C and 190C or slightly before. This is the \"heads\" fraction.\u003c\/li\u003e \u003cli\u003eYou will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to \"self-clean\" the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your \"main body\" fraction. You will see temps between 190-220C during this fraction.\u003c\/li\u003e \u003cli\u003eContinue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed.\u003c\/li\u003e \u003cli\u003eThe final \"tails\" fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The \"tails\" fraction has an obvious color change and will be darker than the \"main body\" fraction. You will see temps between 200-250C during this fraction.\u003c\/li\u003e \u003cli\u003eAs fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well.\u003c\/li\u003e \u003cli\u003eOnce process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation.\u003c\/li\u003e \u003c\/ol\u003e \u003col\u003e\u003c\/ol\u003e \u003cp\u003e\u003cbr\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Note: This entire setup will ship via motor freight.***\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003e*Notice to \u003c\/span\u003e\u003cspan\u003eCustomers\u003c\/span\u003e\u003cspan\u003e: All units are inspected for broken glassware or parts before leaving BVV. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer\u003c\/span\u003e\u003cspan\u003e \u003c\/span\u003e\u003cem\u003e\u003cstrong\u003eMUST contact BVV within 72 hours from carrier delivery to file a claim\u003c\/strong\u003e.\u003c\/em\u003e\u003cspan\u003e If the customer DOES NOT contact BVV within 72 hours from carrier delivery, then BVV cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. \u003c\/span\u003e\u003c\/p\u003e \u003chr\u003e \u003cp\u003e\u003cspan\u003eBVV is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.\u003c\/span\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Standard","offer_id":49567944671543,"sku":"SPTK","price":2350.0,"currency_code":"USD","in_stock":true},{"title":"No Pump","offer_id":49567944704311,"sku":"SPTK-1","price":2100.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/e47a7049cdd10696fcd1c369714a8377.jpg?v=1758128062"},{"product_id":"2l-best-value-electric-lift-rotary-evaporator","title":"BVV - 2L BVV Electric Lift Rotary Evaporator","description":"\u003cp\u003e \u003c\/p\u003e \u003ch1\u003e\u003cspan\u003e\u003cstrong\u003e2L BVV Electric Lift Rotary Evaporator\u003c\/strong\u003e\u003c\/span\u003e\u003c\/h1\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003eThe 2L BVV Electric Lift Rotary Evaporator is the ideal tabletop rotovap for small scale evaporation and recovery of solvents. Designed with ease of use in mind, the 2L allows users to separate solvents from a given mixture with minimal user input. The heating bath and temperature controls allow for precise, repeatable results. The double helix vertical condenser gives maximum surface area for condensation of vapors. PTFE seals on the entire system are made for maximum chemical resistance to ensure vacuum depth and lifespan of the system. Our rotovaps are a fraction of the price of more costly systems with the same functionaility and evaporation efficiency. \u003c\/span\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cimg width=\"100%\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_rotovapflowchart_jpg?4051677996186436891\" alt=\"Rotovap Flow Chart\" title=\"Rotovap Flow Chart\"\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003ch3\u003e\u003cstrong\u003e2L Best Value Electric Lift Rotovap Parts Diagram\u003c\/strong\u003e\u003c\/h3\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003ch3\u003e\u003cstrong\u003e\u003cimg width=\"100%\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0078\/8814\/2451\/t\/2\/assets\/description_image_2Ldiagram_png?2460235208498416581\" alt=\"2L Parts Diagram\" title=\"2L Parts Diagram\"\u003e\u003c\/strong\u003e\u003c\/h3\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cp\u003e\u003cspan\u003e\u003cstrong\u003eFeatures:\u003c\/strong\u003e\u003c\/span\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003eDigital PID temperature and rotation speed control\u003c\/li\u003e \u003cli\u003eAll PTFE valves for improved lifespan and chemical resistance\u003c\/li\u003e \u003cli\u003eDirect injection capability for continuous feeding of solution\u003c\/li\u003e \u003cli\u003eSmall tabletop footprint\u003c\/li\u003e \u003cli\u003eElectric multi-level lifting mechanism for ease of use\u003c\/li\u003e \u003cli\u003eCE Listed\u003c\/li\u003e \u003cli\u003e90-day limited warranty \u003cspan\u003e(excludes glassware, consumables \u0026amp; moving parts)\u003c\/span\u003e \u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003cspan\u003e\u003cstrong\u003eSpecifications:\u003c\/strong\u003e\u003c\/span\u003e\u003c\/p\u003e \u003ctable border=\"1\"\u003e \u003ctbody\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cb\u003eModel\u003c\/b\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e\u003cb\u003e2L Best Value Electric Lift Rotary Evaporator\u003c\/b\u003e\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eOptimum Ambient Temperature\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e5~25C \/ 41~105.8F\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eGlass Material\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003eGG-17 High Borosilicate\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003ePower (V\/Hz)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e110V 60Hz\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eSpeed Regulation\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003eDigital Step-less Regulation\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eRotation Speed\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e20-198 RPM\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eSet Temperature\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e0-99C \/ 0-210F\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eTemperature Control\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003eDigital Temperature Control\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eMaximum Vacuum Pressure\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e-29.8 inHg\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eEvaporating Flask Capacity\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e2L (2000mL)\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eReceiving Flask Capacity\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e1L (1000mL)\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eCondenser Style\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003eVertical Double Helix\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eEvaporation Capacity\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003eAlcohol \u0026gt;\/= 1 L\/H\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eHeater Max Current Draw (Amps)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e13.6\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eWater Bath Material\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003eTeflon Composite\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eWater Bath Size\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e10 x 5 in.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eLifting Function\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003eElectric\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eLifting Stroke\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e14cm \/ 5.5 in.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eTotal Power Consumption (kW)\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e1.8 kW\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eDimensions\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e28 x 18 x 27 in.\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eWeight\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e37.2 kg \/ 82 lbs\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eVacuum Connection\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e3\/8\" Barb\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eCondenser Connection\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e3\/8\" Barb\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eWarranty\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003e90 days excluding glass parts\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003ctr\u003e \u003ctd\u003e \u003cp\u003e\u003cstrong\u003eCertifications\u003c\/strong\u003e\u003c\/p\u003e \u003c\/td\u003e \u003ctd\u003e \u003cp\u003eCE\u003c\/p\u003e \u003c\/td\u003e \u003c\/tr\u003e \u003c\/tbody\u003e \u003c\/table\u003e \u003cp\u003e\u003cb\u003eRotovap Quick Start Guide\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eThis guide gives basic quick start instructions for rotovaps. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs. \u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cbr\u003e\u003c\/p\u003e \u003cul\u003e \u003cli\u003eClean and assemble unit. Make sure all pieces are cleaned and sterilized using an alcohol solution.\u003c\/li\u003e \u003cli\u003eConnect chiller to condenser and set to 0C (32F). Always fill a rotovap condenser from the top down (chiller output to top of condenser, chiller input to bottom of condenser).\u003c\/li\u003e \u003cli\u003eConnect vacuum pump to cold trap and connect cold trap to vacuum port on rotovap.\u003c\/li\u003e \u003cli\u003eTurn on heat bath and set to 40C (113F).\u003c\/li\u003e \u003cli\u003eOnce heat bath, chiller and cold trap have reached desired temperatures, turn on rotovap motor and set speed to approximately 100 RPM (does not have to be precise). Keep in mind, higher RPM's will increase evaporation power but also increase heat load.\u003c\/li\u003e \u003cli\u003eStart vacuum pump and allow vacuum to pull down for a few minutes before injection.\u003c\/li\u003e \u003cli\u003eOnce vacuum has been pulled to a sufficient level (does not have to be precise but should be below 100 Torr), using the injection valve, very slowly inject approximately 500 mL of solution into evaporating flask and then close the valve. Allow this small amount to begin evaporating. You may see the chiller begin to rise in temperature, this is called \"priming\" the rotovap.\u003c\/li\u003e \u003cli\u003eOnce the temperature stops rising or all liquid is almost completely evaporated, open the injection valve again very slowly so that a small amount of liquid begins to enter the evaporating flask. Do not close injection valve this time but continue to allow solution to enter the evaporating flask.\u003c\/li\u003e \u003cli\u003eAt this point you must try to match the input speed to the output speed. What this means is that you should be injecting the same amount of liquid into the rotovap that is equal to the amount of liquid dripping from the condenser into the receiving flask. You will know that the input speed and output speed are matched because the chiller will remain at a stable temperature. If the chiller begins to rise, then you are injecting too much liquid. Dial back the valve until the chiller stabilizes.\u003c\/li\u003e \u003cli\u003eOnce everything is stabilized, you may walk away from the rotovap if necessary. Check every so often to make sure temperatures remain stable and evaporation continues efficiently.\u003c\/li\u003e \u003c\/ul\u003e \u003cp\u003e\u003cstrong\u003e***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer \u003cstrong\u003eMUST \u003c\/strong\u003econtact BVV \u003cstrong\u003ewithin 3 days\u003c\/strong\u003e \u003cstrong\u003eof delivery\u003c\/strong\u003e to file a claim and receive a replacement part. If customer \u003cstrong\u003eDOES NOT\u003c\/strong\u003e contact BVV \u003cstrong\u003ewithin 3 days of delivery\u003c\/strong\u003e responsibility for replacement parts falls on the customer and they must pay for replacement pieces.***\u003c\/strong\u003e\u003c\/p\u003e \u003cp\u003e\u003cstrong\u003e***Glassware Safety Disclaimer: BVV is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***\u003c\/strong\u003e\u003c\/p\u003e","brand":"BVV","offers":[{"title":"Liquid Cooling Coil","offer_id":49567958794551,"sku":"RT2LE","price":1550.0,"currency_code":"USD","in_stock":true},{"title":"Dry Ice Condenser","offer_id":49567958827319,"sku":"RT2LE-DI2LE","price":1650.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0674\/0341\/5863\/files\/2l-bvv-electric-lift-rotary-evaporator-344471.jpg?v=1726549947"}],"url":"https:\/\/www.blacklabelsupply.io\/collections\/xeq-distillation.oembed","provider":"BLACK LABEL","version":"1.0","type":"link"}